Copper-based spherical powder material, as well as preparation method and application thereof
A spherical powder, copper-based technology, applied in the direction of welding/cutting media/materials, manufacturing tools, welding equipment, etc., can solve the problems of low bulk density, low surface tension, poor powder sphericity, etc., to meet the requirements of large welding The effects of seam welding, high bulk density, and high sphericity
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preparation example Construction
[0028] The preparation method of the aforementioned copper-based spherical powder material provided by another aspect of the embodiments of the present invention includes:
[0029] Mix the smelted copper, phosphorus source, tin source, nickel source and reducing agent evenly, and carry out smelting;
[0030] The smelted product is pulverized by water atomization or gas atomization to obtain the copper-based spherical powder material.
[0031] Further, the preparation method includes: first smelting the electrolytic copper, after the metal is melted, and then introducing pure oxygen to the surface of the smelted copper to further remove impurities such as aluminum, titanium and zirconium that may exist in the raw materials.
[0032] Further, the preparation method includes: first covering the surface of the smelted copper with a reducing agent, and then adding phosphorus sources, tin sources, and nickel sources to the smelted copper.
[0033] Further, the reducing agent includ...
Embodiment 1
[0056] 1. Select electrolytic copper plate, pure tin, and phosphorus-copper master alloy with a phosphorus content of 14wt% as alloy raw materials, put the electrolytic copper plate into an intermediate frequency furnace for smelting, and after the metal is melted, inject oxygen into the surface of the molten metal for 10 Minutes to further remove active metal impurities such as aluminum, zirconium, and titanium inside the metal. After the ventilation is finished, put an appropriate amount of charcoal into the molten metal, and add phosphorus copper master alloy, pure tin and pure nickel according to the mass percentage: P content 0.01wt%, Sn content 0.1wt%, Ni content 0.1wt%.
[0057] 2. Take an appropriate amount of material for analysis to detect the impurity content in the alloy. The impurity Al content is 150ppm, the Ti content is 100ppm, and the Zr content is 120ppm.
[0058] 3. After smelting, carry out water atomization milling, adopt ring-hole type water atomization ...
Embodiment 2
[0063] 1. Select electrolytic copper plate, pure tin, and phosphorus-copper master alloy with a phosphorus content of 14wt% as alloy raw materials, put the electrolytic copper plate into an intermediate frequency furnace for smelting, and after the metal is melted, inject oxygen into the surface of the molten metal for 10 Minutes to further remove active metal impurities such as aluminum, zirconium, and titanium inside the metal. After the ventilation is over, put an appropriate amount of charcoal into the molten metal, and add phosphorus copper master alloy, pure tin and pure nickel according to the mass percentage: P content 0.2wt%, Sn content 0.5wt%, Ni content 1wt%.
[0064] 2. Take an appropriate amount of material for analysis to detect the content of impurities and trace elements in the alloy. The impurity Al content is 150ppm, the Ti content is 100ppm, and the Zr content is 120ppm.
[0065] 3. After smelting, carry out water atomization milling, adopt ring-hole type w...
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Abstract
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