A preparation method of electromagnetic shielding material based on boron nitride nanosheet/carbon fiber composite modification
A technology of electromagnetic shielding material and carbon fiber material, applied in shielding materials, magnetic field/electric field shielding, electrical components, etc., can solve the problems of high weight, limitation, decreased corrosion resistance of composite materials, etc., achieve excellent mechanical properties, improve electromagnetic shielding performance effect
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Embodiment 1
[0027] A method for preparing an electromagnetic shielding material based on boron nitride nanosheet / carbon fiber composite modification, comprising the following steps:
[0028] (1) Boron nitride powder and isopropanol are mixed, sonicated at a power of 500W, every 30min of sonication, stop for 10min, then continue sonication, a total of 1h of sonication, after the sonication is finished, a dispersion is obtained; wherein, the nitrogen The dosage ratio of boron powder and isopropanol is 1g: 30ml;
[0029] (2) Add silane coupling agent to the dispersion liquid, stir for 30min under the state of 1500 rev / min, then filter, dry the solid, and make boron nitride nanosheets; wherein, the addition amount of silane coupling agent is isopropyl 3% of alcohol mass;
[0030] (3) carrying out nickel-plating treatment on the surface of boron nitride to obtain boron nitride nanosheets with nickel-plated surface;
[0031] (4) Clean the carbon fiber with acetone, dry it, and then use microw...
Embodiment 2
[0034] A method for preparing an electromagnetic shielding material based on boron nitride nanosheet / carbon fiber composite modification, comprising the following steps:
[0035] (1) Boron nitride powder and isopropanol are mixed, sonicated at a power of 1000W, every 30 minutes of sonication, stop for 10 minutes, and then continue to sonicate for a total of 4 hours of sonication, and a dispersion is obtained after the sonication; wherein, the nitrogen The dosage ratio of boron powder and isopropanol is 1g: 60ml;
[0036] (2) Add silane coupling agent to the dispersion liquid, stir for 30min under the state of 3000 rpm, then filter, dry the solid, and make boron nitride nanosheets; wherein, the addition amount of silane coupling agent is isopropyl 6% of alcohol mass;
[0037] (3) carrying out nickel-plating treatment on the surface of boron nitride to obtain boron nitride nanosheets with nickel-plated surface;
[0038] (4) Clean the carbon fiber with acetone, dry it, and then...
Embodiment 3
[0041] A method for preparing an electromagnetic shielding material based on boron nitride nanosheet / carbon fiber composite modification, comprising the following steps:
[0042] (1) Boron nitride powder and isopropanol were mixed, sonicated at a power of 600W, every 30 minutes of sonication, stopped for 10 minutes, and then continued to sonicate for a total of 1.5 hours of sonication, and a dispersion was obtained after the sonication; wherein, the The dosage ratio of boron nitride powder and isopropanol is 1g: 40ml;
[0043] (2) Add the silane coupling agent to the dispersion liquid, stir for 30min under the state of 2000 rpm, then filter, dry the solid, and make boron nitride nanosheets; wherein, the addition amount of the silane coupling agent is isopropyl 4% of alcohol mass;
[0044](3) carrying out nickel-plating treatment on the surface of boron nitride to obtain boron nitride nanosheets with nickel-plated surface;
[0045] (4) Clean the carbon fiber with acetone, dry...
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