A kind of preparation method of red photon glaze
A photon and red technology, applied in the field of preparation of red photon glaze, can solve the problems of difficulty in large-scale production, increase the uncontrollability of glaze layer structure, and low sintering temperature of colloidal system, achieve high refractive index contrast, and be easy to promote on a large scale , the effect of a broad commercial market
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Embodiment 1
[0021] A preparation method of red photonic glaze, the concrete steps are:
[0022] (1) According to the mass percentage of material composition: kaolin 12.5%, quartz 16.5%, TiO 2 12.5%, limestone 14.5%, albite 15.5%, ZnO 18.5%, talc 10.0%;
[0023] (2) Put the raw materials in step (1) into a ball mill for 1 hour;
[0024] (3) Sieve the glaze slurry milled in step (2) to obtain a glaze slurry with a particle size of <45 μm, and the aging time is 24 hours;
[0025] (4) Applying the processed raw materials in step (3) to the surface of the green body;
[0026] (5) Dry the sample after glazing in step (4) at 60°C for 10 hours;
[0027] (6) Put the sample dried in step (5) into a high-temperature electric furnace for sintering, and then cool naturally with the furnace to obtain a bright red photonic glaze; ℃, the holding time is 30 minutes.
Embodiment 2
[0029] A preparation method of red photonic glaze, the concrete steps are:
[0030] (1) According to the mass percentage of material composition: kaolin 14.0%, quartz 12.5%, TiO 2 18.5%, limestone 9.0%, albite 26.0%, ZnO 12.5%, talc 7.5%;
[0031] (2) Put the raw materials in step (1) into a ball mill for 1 hour;
[0032] (3) Sieve the glaze slurry milled in step (2) to obtain a glaze slurry with a particle size of <45 μm, and the aging time is 24 hours;
[0033] (4) Applying the processed raw materials in step (3) to the surface of the green body;
[0034] (5) Dry the sample after glazing in step (4) at 60°C for 10 hours;
[0035] (6) Put the sample dried in step (5) into a high-temperature electric furnace for sintering, and then cool naturally with the furnace to obtain a bright red photonic glaze; the maximum temperature of the sintering process is 1300 ° C, the holding time is 90 minutes, and the ℃, the holding time is 30 minutes.
Embodiment 3
[0037] A preparation method of red photonic glaze, the concrete steps are:
[0038] (1) According to the mass percentage of material composition: kaolin 15.5%, quartz 15.0%, TiO 2 10.0%, limestone 16.5%, albite 16.5%, ZnO 17.5%, talc 9.0%;
[0039] (2) Put the raw materials in step (1) into a ball mill for 1 hour;
[0040] (3) Sieve the glaze slurry milled in step (2) to obtain a glaze slurry with a particle size of <45 μm, and the aging time is 24 hours;
[0041] (4) Applying the processed raw materials in step (3) to the surface of the green body;
[0042] (5) Dry the sample after glazing in step (4) at 60°C for 10 hours;
[0043] (6) Put the sample dried in step (5) into a high-temperature electric furnace for sintering, and then cool naturally with the furnace to obtain a bright red photonic glaze; ℃, the holding time is 30 minutes.
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