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ASA emulsifying device and control method

An emulsifying device and control method technology, applied in chemical instruments and methods, mixing methods, transportation and packaging, etc., can solve the problem of prone to hydrolysis, alcoholysis and ammonolysis, high maintenance cost of regenerative turbo pump, interference with sizing agent application. It can improve the emulsification effect, retention performance and anti-anion interference performance, and improve the emulsification efficiency.

Inactive Publication Date: 2019-08-02
邱振权
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The Venturi system needs to add a large amount of surfactant to ASA, and the surfactant will interfere with the sizing effect of the sizing agent in the paper; the maintenance cost of the regenerative turbo pump is high, and the production cost is high; the multi-stage centrifugal pump occupies a large area, Low service life, not yet widely used
[0005] In the ASA emulsification control method in the prior art, since the ASA structure contains acid anhydride, hydrolysis, alcoholysis, and ammonolysis are extremely prone to occur. Since ASA requires on-site emulsification, the hardness of the water is relatively high, and impurities such as calcium and magnesium ions in the water Existence, ASA is very prone to hydrolysis; when the emulsifier emulsifies ASA to form an ASA emulsion, the emulsifier such as starch needs to be gelatinized and cooled before use, and the surfactant will bring adverse effects on sizing, and the sizing process is complicated and difficult. control

Method used

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  • ASA emulsifying device and control method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] refer to figure 1 , figure 2 As shown, a kind of ASA emulsification device comprises water treatment device 13, emulsifier pretreatment device, emulsification equipment and controller;

[0041] Described water treatment device 13 comprises water treatment tank inlet 131 and water treatment tank outlet 132, and described water treatment tank outlet is connected with emulsifier pretreatment device and emulsification equipment through tee; Described water treatment device 13 is ion exchange Resin box;

[0042] The emulsifier pretreatment device includes a first static mixer 1, a reactor 2, and a second static mixer 3 connected in series in sequence, the inlet of the first static mixer 1 is connected to the outlet 132 of the water treatment tank, and the first The outlet of the static mixer 1 is connected to the reactor 2; the reactor 2 is also connected to a second static mixer 3; the outlet of the second static mixer 3 is connected to the emulsifier pump 10 of the emul...

Embodiment 2

[0054] The difference between this embodiment and embodiment 1 is that the specific steps of the method for controlling emulsification of ASA are as follows:

[0055] Step 1, water pretreatment: water enters the water treatment device from the inlet of the water treatment tank, and the water whose hardness is reduced by ion exchange resin is pumped out from the outlet of the water treatment tank, and then pumped into the emulsifier pretreatment device and emulsification equipment through the water pump ;

[0056] Step 2, emulsifier pretreatment, the emulsifier is pre-filled in the first static mixer, and the emulsifier is an amphiphilic emulsifier; the pretreated water is mixed with the emulsifier through the first static mixer, Entering the reactor under water drive; the emulsifier aqueous solution after the reaction enters the emulsifier pump from the second static mixer, and the emulsifier is processed into an emulsifier aqueous solution;

[0057] Step 3, emulsifier treatm...

Embodiment 3

[0063] The difference between this embodiment and embodiment 1 is that the specific steps of the method for controlling emulsification of ASA are as follows:

[0064] Step 1, water pretreatment: water enters the water treatment device from the inlet of the water treatment tank, and the water whose hardness is reduced by ion exchange resin is pumped out from the outlet of the water treatment tank, and then pumped into the emulsifier pretreatment device and emulsification equipment through the water pump ;

[0065] Step 2, emulsifier pretreatment, the emulsifier is pre-filled in the first static mixer, and the emulsifier is an amphiphilic emulsifier; the pretreated water is mixed with the emulsifier through the first static mixer, Entering the reactor under water drive; the emulsifier aqueous solution after the reaction enters the emulsifier pump from the second static mixer, and the emulsifier is processed into an emulsifier aqueous solution;

[0066] Step 3, emulsifier treatm...

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Abstract

The invention belongs to the technical field of emulsifying devices, and particularly relates to an ASA emulsifying device and a control method. The emulsifying device comprises a water treatment device, an emulsifying agent pretreating device, emulsifying equipment and a controller, wherein the emulsifying agent pretreating device comprises a first static mixer, a reactor and a second static mixer which are sequentially connected serially; the emulsifying equipment comprises an emulsifying agent pump, a sizing agent pump, an emulsifying pump, an acid pump and a water pump; the emulsifying equipment further comprises a circulating pipeline; the controller is in communication connection with a pH meter, a pressure sensor and a temperature sensor. The control method adopting the ASA emulsifying device comprises the following steps: pretreating water, pretreating an emulsifying agent, treating the emulsifying agent, mixing ASA and the emulsifying agent, performing primarydilution and performing secondary dilution. The ASA emulsifying device is simple in structure, convenient and fast to operate and stable and reliable in technology, and reduces the hydrolysis degree of a sizing agent.

Description

technical field [0001] The invention belongs to the technical field of emulsification devices, and in particular relates to an ASA emulsification device and a control method. Background technique [0002] Sizing makes paper or board liquid-resistant, more suitable for writing or moisture-resistant. The sizing of paper is mainly determined by three sub-processes: the retention of sizing particles on the surface of fibers and fillers; the spreading and redistribution of sizing on the surface of fibers and fillers; the fixation of sizing on the surfaces of fibers and fillers. To have a good sizing effect, it is necessary to ensure that the sizing agent is well spread on the fiber surface. [0003] Alkenyl succinic anhydride (ASA) is a reactive neutral / alkaline sizing agent that is an oily liquid at room temperature and is widely used due to its high activity, low sizing cost, and fast curing rate. However, ASA is insoluble in water, and can be evenly dispersed in the paper ma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01F3/08B01F3/20B01F13/10B01F15/00B01F15/06B01F23/70
CPCB01F23/4105B01F23/70B01F23/708B01F33/834B01F33/82B01F33/85B01F33/8362B01F35/2113B01F35/2115B01F35/2132B01F35/221B01F35/2213B01F35/2209B01F35/2215B01F35/187B01F2035/98B01F2035/99B01F35/92
Inventor 邱振权
Owner 邱振权
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