Modified graphene heat radiation paint, and preparation method thereof
A technology of heat-dissipating coatings and graphene, which is applied in anti-corrosion coatings, coatings, etc., can solve the problems of small thermal conductivity of thermally conductive adhesives, difficulty in achieving heat dissipation, and limited use occasions, achieving stable performance and facilitating large-scale promotion. The effect of improving stability and service life
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Embodiment 1
[0034] A modified graphene heat-dissipating coating, comprising the following raw materials in parts by weight: 70 parts of silicone resin, 20 parts of modified graphene powder, 5 parts of inorganic filler, 1.5 parts of curing agent, 12 parts of solvent, 3 parts of dispersant and Leveling agent 3 parts.
[0035] The silicone resin can be cross-linked to form a network chemical structure. The silicone resin is Xilikang silicone rubber.
[0036] The modified graphene powder adopts the modified compound as silane coupling agent KH570.
[0037] The inorganic filler is silicon carbide.
[0038] The solvent is simethicone.
[0039] A preparation method of a modified graphene heat-dissipating coating, comprising the steps of: A, mechanically exfoliating graphite powder to prepare a graphene slurry, which is dried into a graphene powder for subsequent use; B, chemically modified graphene, dried into a powder body, for subsequent use; C, the modified graphene powder in the organosi...
Embodiment 2
[0046] The difference between this embodiment and the above-mentioned embodiment 1 is:
[0047] A modified graphene heat-dissipating coating, comprising the following raw materials in parts by weight: 70 parts of silicone resin, 20 parts of modified graphene powder, 5 parts of inorganic filler, 1.5 parts of curing agent, 12 parts of solvent, 3 parts of dispersant and Leveling agent 3 parts.
[0048] The modified graphene powder adopts titanate coupling agent Ti201 as a modification compound.
[0049] The inorganic filler is silicon nitride.
[0050] The solvent is N,N-dimethylformamide.
[0051] The step A is specifically: take 1 weight part of flake graphite, mix it with 5 weight parts of deionized water, add 0.01 weight part of SDBS dispersant with a mass fraction of 1%, and use a sand mill under the condition of 2000r / min The graphene slurry was prepared by mechanical exfoliation for 6 hours, washed with deionized water for several times, then suction-filtered, and dried i...
Embodiment 3
[0056] A modified graphene heat dissipation coating, comprising the following raw materials in parts by weight: 50 parts of silicone resin, 1 part of modified graphene powder, 1 part of inorganic filler, 1 part of curing agent, 5 parts of solvent, 1 part of dispersant and Leveling agent 1 part.
[0057] The modified graphene powder uses a modified compound as an aluminate coupling agent.
[0058] The inorganic filler is silicon powder.
[0059] The solvent is N,N-dimethylformamide.
[0060] The step A is specifically: take 0.8 parts by weight of flake graphite, mix it with 3 parts by weight of deionized water, add 0.005 parts by weight of SDBS dispersant with a mass fraction of 0.5%, and use a sand mill under the condition of 1500r / min The graphene slurry was prepared by mechanical exfoliation for 8 hours, washed with deionized water several times, then suction-filtered, and dried in a vacuum oven to form graphene powder; wherein, the particle size of the flake graphite was ...
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