Method for preparing high-silicon steel sheet through powder rolling

A technology of powder rolling and high-silicon steel, applied in the direction of manufacturing tools, heat treatment equipment, metal processing equipment, etc., can solve problems such as difficulty in applying industrial production, restricting production and application, poor processing performance, etc., and achieve industrial production and production efficiency Effect of high and improved roll formability

Active Publication Date: 2019-10-22
UNIV OF SCI & TECH BEIJING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Although 6.5% Si silicon steel has excellent magnetic properties and wide application prospects, 6.5% Si high silicon steel is brittle in texture and poor in processability, making it difficult to prepare by conventional rolling methods, thus restricting its production and application
However, although the above methods avoid or solve the problem of difficult deformation of the alloy to a certain extent, they only stay in the laboratory research stage and are difficult to apply to industrial production.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment example 1

[0029] (1) In the process of preparing carbonyl iron powder, add Si powder with a particle size of ≤20um, wherein the mass of silicon powder is twice that of iron powder, and prepare silicon powder coated with carbonyl iron powder, that is, SF powder.

[0030] (2) Mix the -325 mesh electrolytic iron powder and the prepared SF powder according to the ratio of mass fraction 120:13 to form a mixed powder of Fe-6.5% Si, and mix the above powder for 0.5h with a v-type mixer;

[0031] (3) Using Russian two-roller 45° inclined rolling mill, using the friction between the roll and the powder to feed the material, the rolled product has a thickness of 1.2mm, a width of 80mm, and a density of 6.22g / cm 3 green sheet;

[0032] (4) The green sheets are separated by ceramic sheets, and vacuum sintered at 1300°C for 2 hours to achieve metallurgical bonding and uniform element diffusion;

[0033] (5) After the above-mentioned sintered slab is heated to 930° C., hot rolling is carried out 6 t...

Embodiment example 2

[0037] (1) In the process of preparing carbonyl iron powder, add Si powder with a particle size of ≤20um, wherein the mass of silicon powder is 4 times that of iron powder, and prepare silicon powder coated with carbonyl iron powder, that is, SF powder.

[0038] (2) Mix the -325 mesh electrolytic iron powder and the prepared SF powder according to the ratio of mass fraction 147:13 to form a mixed powder of Fe-6.5% Si, and mix the above powder for 2 hours by using a v-type mixer;

[0039] (3) Using a Russian two-roller 45° inclined rolling mill, using the friction between the roll and the powder to feed, the rolled product has a thickness of 1.0mm, a width of 160mm, and a density of 6.41g / cm 3 green sheet;

[0040] (4) The green sheets are separated by ceramic sheets, and vacuum sintered at 1350°C for 1 hour to achieve metallurgical bonding and uniform element diffusion;

[0041] (5) After the above-mentioned sintered slab is heated to 850° C., hot rolling is carried out 8 tim...

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Abstract

The invention discloses a method for preparing a high-silicon steel sheet through powder rolling, and belongs to the technical field of powder metallurgy. The method comprises the following steps thatelectrolytic iron powder and silicon powder coated with iron powder are adopted, the raw materials are simply mixed through a v-shaped mixer to form Fe-6.5wt.%Si. A green sheet is formed through a powder rolling method, is subjected to high-temperature sintering so as to be subjected to metallurgical bonding, and is subjected to multi-pass hot rolling to a certain thickness and then is subjectedto cold rolling for 2-4 times, and finally annealing is carried out at a high temperature to obtain the high-silicon steel sheet with excellent performance. By adopting the powder rolling method, theprocess flow for preparing the sheet can be effectively shortened, the formability of a powder system is greatly improved by adopting the silicon powder coated with the iron powder in raw materials, so that the process complexity and the subsequent debinding residual carbon problem caused by addition of a forming agent are avoided, and the method has the advantages of being simple to operate, highin production efficiency, high in product precision, free of pollution and included foreign materials, excellent in performance and the like.

Description

technical field [0001] The invention belongs to the technical field of powder metallurgy, and relates to a method for preparing high-silicon steel flakes through powder rolling. Background technique [0002] Magnetic materials are mainly divided into two categories: permanent magnets and soft magnetic materials. Permanent magnetic materials are mainly used to provide stable magnetic fields, information storage, etc., and soft magnetic materials are mainly used for electric energy conversion and electromagnetic signal conversion in the power electronics industry. The remanence and coercivity of soft magnetic materials are very small, and they are easily magnetized repeatedly in a magnetic field. When the external magnetic field is removed, most or all of the obtained magnetism will be lost, so they have been widely used in electrical equipment and electronic equipment. The development of traditional soft magnetic materials has gone through the process from pure iron, silicon...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F3/18B22F1/02B22F3/10B22F3/24C21D1/26C21D1/773C21D6/00C21D8/12C21D9/46
CPCB22F3/18B22F3/1007B22F3/24C21D1/26C21D1/773C21D6/008C21D8/1216C21D9/46B22F2003/248B22F1/17
Inventor 杨芳秦乾郭志猛孙海霞隋延力邵艳茹林圣增路新陈存广李沛陈明训魏家树
Owner UNIV OF SCI & TECH BEIJING
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