Activated carbon composite material for sewage treatment and preparation method thereof
A composite material and sewage treatment technology, applied in water/sewage treatment, adsorbed water/sewage treatment, water/sludge/sewage treatment, etc. Adsorption capacity, to achieve the effect of adsorption
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Embodiment 1
[0030] The preparation of embodiment 1 modified activated carbon
[0031] (1) Activated carbon is placed in 6mol / L nitric acid solution, heated to reflux for 5h, then washed with water until neutral, and dried to obtain carboxylated activated carbon;
[0032] (2) Add carboxylated activated carbon and sorbitol to the organic solvent propylene glycol and mix, then add catalyst DCC, carry out heating and reflux reaction for 12h, the product is washed with water, and after drying, sorbitol grafted activated carbon is obtained; wherein carboxylated activated carbon and sorbitol The weight ratio of sugar alcohol is 1:8; the dosage ratio of carboxylated activated carbon and organic solvent propylene glycol is 1g:20mL; the dosage ratio of carboxylated activated carbon and catalyst DCC is 1:0.8;
[0033] (3) Get sorbitol grafted activated carbon and rosin and add in the organic solvent ethanol and mix, then add catalyst zinc oxide, carry out heating and reflux reaction 10h, the product...
Embodiment 2
[0039] The preparation of embodiment 2 modified active carbons
[0040] (1) Activated carbon is placed in 5mol / L nitric acid solution, heated to reflux for 6h, then washed with water until neutral, and dried to obtain carboxylated activated carbon;
[0041](2) Add carboxylated activated carbon and sorbitol to the organic solvent propylene glycol and mix, then add catalyst DCC, carry out heating and reflux reaction for 16h, the product is washed with water, and after drying, sorbitol grafted activated carbon is obtained; wherein carboxylated activated carbon and sorbitol The weight ratio of sugar alcohol is 1:6; the dosage ratio of carboxylated activated carbon and organic solvent propylene glycol is 1g:15mL; the dosage ratio of carboxylated activated carbon and catalyst DCC is 1:0.5;
[0042] (3) Get sorbitol grafted activated carbon and rosin and add in the organic solvent ethanol and mix, then add catalyst zinc oxide, carry out heating and reflux reaction 8h, the product is ...
Embodiment 3
[0045] The preparation of embodiment 3 modified active carbons
[0046] (1) Activated carbon is placed in 8mol / L nitric acid solution, heated to reflux for 4h, then washed with water until neutral, and dried to obtain carboxylated activated carbon;
[0047] (2) Add carboxylated activated carbon and sorbitol to the organic solvent propylene glycol and mix, then add catalyst DCC, carry out heating and reflux reaction for 10h, the product is washed with water, and after drying, sorbitol grafted activated carbon is obtained; wherein carboxylated activated carbon and sorbitol The weight ratio of sugar alcohol is 1:10; the dosage ratio of carboxylated activated carbon and organic solvent propylene glycol is 1g:25mL; the dosage ratio of carboxylated activated carbon and catalyst DCC is 1:1;
[0048] (3) Get sorbitol grafted activated carbon and rosin and add in the organic solvent ethanol and mix, then add catalyst zinc oxide, carry out heating and reflux reaction 12h, the product is...
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