A method for recovering drilling cuttings and its products and applications
A technology for recycling and drilling cuttings, applied in earthwork drilling, flushing boreholes, boreholes/well components, etc., can solve the problem of poor harmless treatment effect, increase the compactness of cuttings particles, water resistance and chemical resistance Corrosion, poor performance of recycled products, etc., to achieve strong flocculation and chemical reaction capabilities, improve erosion resistance and water resistance, reduce temperature shrinkage and dry shrinkage cracking
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preparation example Construction
[0032] Concrete preparation method comprises the following steps:
[0033] (1) Prepare tert-butanol peroxide with ethanol aqueous solution to make a mixed solution A with a mass fraction of 15%;
[0034] (2) Add allyl glycidyl ether to 500 parts of water and mix evenly, then add chlorosilane, and carry out hydrolysis reaction at a temperature of 20°C for 20 minutes. After the hydrolysis is completed, a mixed solution B is obtained;
[0035] (3) Add aluminum sulfate and ferric sulfate to the mixed solution B, stir and dissolve to obtain the mixed solution C;
[0036] (4) Add mixed solution A to mixed solution C at a speed of 80ml / min, and carry out oxidation and co-condensation reaction for 8 hours under the conditions of stirring speed of 50r / min and temperature of 40°C to obtain solution D;
[0037] (5) After the solution D was filtered, it was dried at a temperature of 80° C. to obtain a recovery treatment agent with a water content of 8%.
[0038] In the specific embodiment...
Embodiment 1
[0040] (1) Add 3kg of recovery treatment agent to 100kg of drilling cuttings, stir and react at a speed of 55r / min for 1.5h to obtain a mixed solution;
[0041] (2) Centrifuge the mixed solution to obtain sediment and clarified solution;
[0042] (3) Dry and solidify the precipitate at a temperature of 110° C. for 15 minutes, and then sieve to obtain a solid particle product.
Embodiment 2
[0044] (1) Add 0.5kg of recovery treatment agent to 100kg of drilling cuttings, stir and react for 1h at a speed of 60r / min to obtain a mixed solution;
[0045] (2) Centrifuge the mixed solution to obtain sediment and clarified solution;
[0046] (3) Dry the precipitate at a temperature of 80°C for 30 minutes, then pulverize and sieve through a pulverizer to obtain solid particles.
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