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Viscoelastic acid-resisting clean fracturing fluid and preparation method thereof

A clean fracturing fluid and viscoelastic technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of joint operations, poor temperature resistance, acid resistance, etc., to reduce reservoir damage and excellent viscoelasticity , the effect of easy compounding

Inactive Publication Date: 2019-11-05
巴州科邦石油助剂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Conventional fracturing fluids usually use guar gum fracturing fluid systems cross-linked in alkaline environments. Disadvantages of being thorough and unable to work in conjunction with acidification and acid fracturing
Although the clean fracturing fluids currently on the market have reduced reservoir damage, they still have disadvantages such as poor temperature resistance, high cost of use, and acid resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] The viscoelastic acid-resistant cleaning fracturing fluid of this embodiment is suitable for 60°C formation viscoelastic acid-resistant cleaning fracturing fluid formula:

[0037] Hydrophobic associating polymer thickener 0.25%, viscoelastic surfactant 2.0%, ammonium chloride 5%, gel breaker is sodium persulfate 0.05%, and the rest is water.

[0038] The hydrophobic associative polymer thickener is a copolymer of acrylamide, acrylic acid, 2-methyl-2-acrylamidopropanesulfonic acid and 14-18 alkyl amide, and the use concentration is 0.3% by mass percentage .

[0039] The viscoelastic surfactant is fatty acid amide betaine, and its use concentration is 2% in terms of mass percentage.

[0040] The inorganic salt is ammonium chloride, and its use concentration is 3% in terms of mass percentage.

[0041] The gel breaker is sodium persulfate, and its use concentration is 0.02% in terms of mass percentage.

[0042] The acid-resistant cleaning fracturing fluid is slightly acidic and has a...

Embodiment 2

[0048] The viscoelastic acid-resistant cleaning fracturing fluid of this embodiment is suitable for 100°C formation viscoelastic acid-resistant cleaning fracturing fluid formulation:

[0049] Hydrophobic associating polymer thickener 0.4%, viscoelastic surfactant 3.0%, ammonium chloride 6%, gel breaker is sodium persulfate 0.05%, and the rest is water.

[0050] The hydrophobically associating polymer thickener is a copolymer of acrylamide, acrylic acid, 2-methyl-2-acrylamidopropanesulfonic acid and 14-18 alkyl amide, and the use concentration is 0.4%.

[0051] The viscoelastic surfactant is fatty acid amide betaine, and its use concentration is 3% in terms of mass percentage.

[0052] The inorganic salt is a mixture of ammonium chloride and sodium chloride, and its use concentration is 4% by mass percentage. In the mixture, the ammonium chloride concentration is not less than 2% by mass percentage.

[0053] The gel breaker is sodium persulfate, and its use concentration is 0.1% in terms...

Embodiment 3

[0060] The viscoelastic acid-resistant cleaning fracturing fluid of this embodiment, which is suitable for formation at 70°C, includes the following components in terms of mass percentage:

[0061] Hydrophobic associating polymer thickener 0.2%, viscoelastic surfactant 2.5%, inorganic salt 3%, gel breaker 0.02%, and the rest is water.

[0062] Wherein, the hydrophobically associating polymer thickener is a copolymer of acrylamide, acrylic acid, 2-methyl-2-acrylamidopropanesulfonic acid and 14-18 alkylamide, and the use concentration is 0.35%.

[0063] The viscoelastic surfactant is fatty acid amide betaine, and its use concentration is 2.7% in terms of mass percentage.

[0064] The inorganic salt is a mixture of ammonium chloride, sodium chloride and potassium chloride, and its use concentration is 5% by mass percentage, and the ammonium chloride concentration in the mixture is not less than 2% by mass percentage.

[0065] The gel breaker is ammonium persulfate, and its use concentratio...

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Abstract

The invention provides a viscoelastic acid-resisting clean fracturing fluid. The acid-resisting clean fracturing fluid is suitable for a stratum of 60-100 DEG C, and the acid-resisting clean fracturing fluid is characterized by comprising, by mass, 0.2-0.4% of a hydrophobic associating polymer thickening agent, 2-3% of a viscoelastic surface active agent, 3-6% of inorganic salt, 0.02-0.2% of a gelbreaker and the balance water. The preparation method comprises the steps of (1), preparation of a base solution, wherein according to the ratio in the formula, the hydrophobic associating polymer thickening agent is prepared into powder and carried by water via negative pressure into a liquid preparation tank, stirring is conducted for about 20-40 minutes, so that the hydrophobic associating polymer thickening agent is swelled, the inorganic salt is added, stirring is conducted to make the inorganic salt completely dissolved, and standing is conducted for 2-3 hours for use; (2), preparationof a surface active agent crosslinking solution, wherein according to the ratio in the formula, the surface active agent and the water are added, and stirring is conducted until the active agent is dissolved completely; (3), preparation of the viscoelastic acid-resisting clean fracturing fluid, wherein the prepared base solution and the prepared surface active agent crosslinking solution are obtained, prepared in a weight ratio of (8-12):1 and significantly stirred to be uniform to obtain the viscoelastic acid-resisting clean fracturing fluid. After 1-3% of HCl is added into a fracturing fluidsystem, the viscosity is reduced by 5% or below.

Description

Technical field [0001] The invention relates to a viscoelastic acid-resistant cleaning fracturing fluid and a preparation method thereof. Background technique [0002] Conventional fracturing fluids usually use guar gum fracturing fluid systems that are cross-linked in an alkaline environment. This type of system has a high cost, and when applied to low-permeability reservoirs, the residual gel will cause greater damage to the formation, and the reservoir will not break the gel. The shortcomings of being thorough, unable to work with acidification and acid fracturing. Although the current clean fracturing fluids on the market have reduced reservoir damage, they still have disadvantages such as poor temperature resistance, high use cost, and acid resistance. Summary of the invention [0003] The technical problem to be solved by the present invention is to provide a formulation of viscoelastic acid-resistant cleaning fracturing fluid prepared by using hydrophobically associating p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68C09K8/88
CPCC09K8/68C09K8/882
Inventor 王铁成曲国玺
Owner 巴州科邦石油助剂有限公司
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