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An aging method to improve the dimensional stability of tic-cr-mo steel matrix composites

A dimensional stability, tic-cr-mo technology, applied in the aging field of improving the dimensional stability of TiC-Cr-Mo steel matrix composites, can solve problems such as stress concentration, affecting material compactness, stable and reliable performance, and cracking

Active Publication Date: 2021-04-23
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in order to improve the dimensional stability of TiC-Cr-Mo steel matrix composites treated by conventional methods, the method of single heat treatment or ultrasonic vibration still has the following disadvantages: 1. Due to the hard phase TiC particles in the composite material and the steel There is a large difference in the elastic modulus between the substrates, which is easy to cause stress concentration at the interface and cause cracking, which affects the compactness of the material and the stability and reliability of the performance. Therefore, a single treatment method cannot take into account the stability of the material structure and stress at the same time; 2 .Improving the dimensional stability of the material is the result of the combination of the stability of the material microstructure and the elimination of residual stress. Although a relatively stable microstructure can be obtained through heat treatment, there are still certain limitations in effectively eliminating the residual stress inside the material. sex

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  • An aging method to improve the dimensional stability of tic-cr-mo steel matrix composites
  • An aging method to improve the dimensional stability of tic-cr-mo steel matrix composites

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] First, place the TiC-Cr-Mo steel-based alloy sample in an ultrasonic device with distilled water as the ultrasonic medium for heating and ultrasonic vibration treatment, wherein the heating temperature is 80°C, the vibration time is 60min, the vibration frequency is 40kHz, and the power is 240W; Immediately after the heating and ultrasonic treatment, the TiC-Cr-Mo alloy sample was placed in an ultrasonic equipment with liquid nitrogen as the ultrasonic medium for ultrasonic vibration treatment, wherein the cooling temperature was -196°C, the vibration time was 120min, and the vibration frequency was 40kHz , the power is 240W; according to the above process cycle 6 times, the treated TiC-Cr-Mo alloy sample is obtained.

[0017] The residual stress on the surface of the alloy obtained in this embodiment is -9MPa, the hardness of the alloy is 1042HV, and the magnetic saturation intensity is 93emu / g. Measure the dimensional change rate of the obtained product after it is pla...

Embodiment 2

[0021] First, place the TiC-Cr-Mo steel-based alloy sample in an ultrasonic device with distilled water as the ultrasonic medium for heating and ultrasonic vibration treatment. The heating temperature is 100°C, the vibration time is 180min, the vibration frequency is 40kHz, and the power is 240W; Immediately after the heating and ultrasonic treatment, the TiC-Cr-Mo alloy sample was placed in an ultrasonic equipment with liquid nitrogen as the ultrasonic medium for ultrasonic vibration treatment, wherein the cooling temperature was -196°C, the vibration time was 240min, and the vibration frequency was 40kHz. The power is 240W; the above-mentioned process is cycled 4 times to obtain the treated TiC-Cr-Mo alloy sample.

[0022] The residual stress on the surface of the alloy obtained in this embodiment is 11MPa, the hardness of the alloy is 1098HV, and the magnetic saturation intensity is 97emu / g. Measure the dimensional change rate of the obtained product after being placed at ro...

Embodiment 3

[0024] First, place the TiC-Cr-Mo steel-based alloy sample in an ultrasonic device with distilled water as the ultrasonic medium for heating and ultrasonic vibration treatment. The heating temperature is 100°C, the vibration time is 240min, the vibration frequency is 40kHz, and the power is 240W; Immediately after the heating and ultrasonic treatment, the TiC-Cr-Mo alloy sample was placed in an ultrasonic equipment with liquid nitrogen as the ultrasonic medium for ultrasonic vibration treatment, wherein the cooling temperature was -196°C, the vibration time was 300min, and the vibration frequency was 40kHz , the power is 240W; according to the above process cycle 8 times, the processed TiC-Cr-Mo alloy sample is obtained.

[0025] The residual stress on the surface of the alloy obtained in this embodiment is 23MPa, the hardness of the alloy is 1134HV, and the magnetic saturation intensity is 112emu / g. Measure the dimensional change rate of the obtained product after being placed...

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Abstract

The invention discloses an aging method for improving the dimensional stability of a TiC-Cr-Mo steel-based composite material, comprising the following steps: heating and ultrasonically aging a TiC-Cr-Mo alloy sample, and then performing liquid nitrogen ultrasonic aging, according to the process The alloy sample is subjected to cooling and heating cycles combined with ultrasonic vibration to obtain a dimensionally stable alloy sample. The present invention can significantly improve the structural stability of the TiC-Cr-Mo steel-based composite material by synergizing the ultrasonic vibration through the cooling and heating cycle, reduce the residual stress inside the composite material, and finally improve the dimensional stability of the TiC-Cr-Mo alloy. Compared with the alloy obtained by the conventional treatment method, the TiC-Cr-Mo steel-based composite material obtained by the method of the present invention reduces the residual stress on the alloy surface from -250 to -200MPa to -10 to 30MPa, and the hardness of the alloy is from 900 to 940HV Increase to 1000 ~ 1200HV.

Description

technical field [0001] The invention belongs to the technical field of composite material processing, and in particular relates to an aging method for improving the dimensional stability of a TiC-Cr-Mo steel-based composite material. Background technique [0002] TiC-Cr-Mo steel-based composite materials mainly use TiC as the hard phase and chromium-molybdenum low-alloy steel as the matrix. The content of the hard phase TiC is 35wt.%, and the content of Cr and Mo is 2wt.%. Generally, after sintering, After forging, annealing and tempering a series of conventional treatments, it can be used to prepare dynamic pressure air bearings, cold working dies, measuring fixtures, etc. in navigation systems. Such parts need to maintain their materials during long-term stable and reliable use. stability of organizational performance. The main factors affecting the stability of material structure and performance are the evolution of the microstructure of the material during the preparati...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21D6/04C21D1/04
CPCC21D1/04C21D6/002C21D6/04
Inventor 肖来荣涂晓萱赵小军蔡圳阳谭威
Owner CENT SOUTH UNIV