Organosilicone master batch, self-cleaning PERT floor heating pipe and preparation method of self-cleaning PERT floor heating pipe
An organic silicone and masterbatch technology, applied in chemical instruments and methods, mechanical equipment, hoses, etc., can solve problems such as reducing the thermal conductivity of pipes, reducing the flow rate of hot water in pipes, and poor flexibility.
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[0035] In the present invention, in terms of parts by weight, the raw materials for the preparation of the organosilicone masterbatch include 40-60 parts of organosilicone powder, preferably 50 parts. In the present invention, the particle size of the organic silicone powder is preferably 2-10 μm, more preferably 6 μm. In the present invention, the preparation method of the organic silicone powder preferably comprises the following steps:
[0036] (1) Provide a dispersion containing surfactant;
[0037] (2) mixing the dispersion liquid described in step (1) with silicone oil and a catalyst to undergo a crosslinking reaction to obtain an organosilicone emulsion;
[0038] (3) The organic silicone emulsion is sequentially filtered, washed, dried and sieved to obtain organic silicone powder.
[0039] The present invention preferably provides a surfactant-containing dispersion. In the present invention, the specific preparation method of the surfactant-containing dispersion is p...
Embodiment 1
[0070] A. Preparation of silicone masterbatch
[0071] (1) At room temperature, in 900g of water, add 40g of sodium alkylbenzene sulfonate, 10g of sodium lauryl sulfate, adjust the pH value to 6 with hydrochloric acid with a mass concentration of 25%, and stir electromagnetically for 10 minutes to obtain a surface-containing Dispersions of active agents;
[0072] (2) Add 1.5g of tetramethylammonium hydroxide, 320g of amino silicone oil, and 208g of methyl silicone oil into the surfactant-containing dispersion obtained in step (1), and use a high stirrer at a constant temperature of 50°C. Stir at a speed of 1350rpm for 28min, then turn to a slow speed, stir at a speed of 230rpm for 9h, and store it at room temperature for 50h, so that the silicone oil is cross-linked and solidified in the dispersion liquid containing a surfactant, and an organic compound that is matured and dispersed evenly is obtained. Silicone emulsion;
[0073] (3) Filter the organosilicone emulsion after ...
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