High-temperature-resistant UV visbreaking adhesive tape

A technology of high temperature resistance and adhesive tape, which is applied in the direction of adhesives, film/sheet adhesives, film/sheet release liners, etc. It can solve the problems of easy precipitation, poor miscibility of resin and masterbatch, poor temperature resistance, etc. , to achieve the effect of not easy to precipitate, increase initial viscosity, and small growth at high temperature

Inactive Publication Date: 2019-11-22
KUNSHAN BYE MACROMOLECULE MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional preparation method of UV viscosifying adhesive is usually realized by adding multifunctional UV resin to high-viscosity acrylic glue. This method has the characteristics of poor miscibility between resin and masterbatch, easy precipitation, and poor temperature resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The invention provides the following technical solutions: a high-temperature resistant UV adhesive tape, comprising a release film layer, a UV adhesive layer, a bottom coating, a flexible substrate layer and a UV active coating arranged sequentially from bottom to top. It is characterized in that: the UV viscosifying adhesive is made of the following raw materials in parts by weight:

[0022] 20 parts of cured resin, 25 parts of methacrylic acid, 5 parts of 2-hydroxy-2-methyl-1-phenyl-1-propanone; 45 parts of methyl trimethyl acetate, 45 parts of diethylene glycol monovinyl ether , 0.5 part of azobisisoheptanonitrile, 4 parts of trimethylolpropane tricrosslinking agent, 0.8 part of isophorone diamine, 0.3 part of anti-aging agent 4010NA, 2 parts of methyl acetate.

[0023] The above-mentioned UV visbreaking adhesive preparation method in the high temperature resistant UV visbreaking adhesive tape comprises the following steps:

[0024] S1. Mix 20 parts of cured resin a...

Embodiment 2

[0034] The invention provides the following technical solutions: a high-temperature resistant UV adhesive tape, comprising a release film layer, a UV adhesive layer, a bottom coating, a flexible substrate layer and a UV active coating arranged sequentially from bottom to top. It is characterized in that: the UV viscosifying adhesive is made of the following raw materials in parts by weight:

[0035] 30 parts of cured resin, 35 parts of methacrylic acid, 9 parts of 2-hydroxy-2-methyl-1-phenyl-1-propanone; 50 parts of methyl trimethyl acetate, 55 parts of diethylene glycol monovinyl ether , 1 part of azobisisoheptanonitrile, 8 parts of trimethylolpropane tricrosslinking agent, 1.5 parts of isophorone diamine, 0.8 part of antioxidant 4010NA, and 8 parts of methyl acetate.

[0036] The above-mentioned UV visbreaking adhesive preparation method in the high temperature resistant UV visbreaking adhesive tape comprises the following steps:

[0037] S1. Mix 30 parts of cured resin and...

Embodiment 3

[0047] The invention provides the following technical solutions: a high-temperature resistant UV adhesive tape, comprising a release film layer, a UV adhesive layer, a bottom coating, a flexible substrate layer and a UV active coating arranged sequentially from bottom to top. It is characterized in that: the UV viscosifying adhesive is made of the following raw materials in parts by weight:

[0048] 21 parts of cured resin, 26 parts of methacrylic acid, 6 parts of 2-hydroxy-2-methyl-1-phenyl-1-propanone; 46 parts of methyl trimethyl acetate, 46 parts of diethylene glycol monovinyl ether , 0.6 parts of azobisisoheptanonitrile, 5 parts of trimethylolpropane tricrosslinking agent, 0.9 parts of isophorone diamine, 0.4 parts of antioxidant 4010NA, and 3 parts of methyl acetate.

[0049] The above-mentioned UV visbreaking adhesive preparation method in the high temperature resistant UV visbreaking adhesive tape comprises the following steps:

[0050] S1. Mix 21 parts of cured resin...

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Abstract

The invention belongs to the technical field of visbreaking adhesive tapes. The invention relates to a high-temperature-resistant UV visbreaking adhesive tape. The UV visbreaking adhesive tape comprises a release film layer, a UV visbreaking adhesive layer, a bottom coating, a flexible base material layer and a UV active coating which are sequentially arranged from bottom to top, and is characterized in that: the UV visbreaking adhesive is prepared from the following raw materials in parts by weight: 20-30 parts of cured resin, 25-35 parts of methacrylic acid and 5-9 parts of 2-hydroxyl-2-methyl-1-phenyl-1-acetone, 45-50 parts of diethylene glycol monovinyl ether, 0.5-1 part of azodiisoheptonitrile and 4-8 parts of a trimethylolpropane tri-crosslinking agent; after UV illumination, the stripping force can be reduced from original 1600 gf / 25mm to 20 gf / 25mm or below; the prepared adhesive tape has the advantages of no pollution, no residue, difficult precipitation, realization of high temperature resistance at 150 DEG C for 1h, substantial improvement of the initial adhesion of the glue, and suitableness for a plurality of coating modes; and the product obtained after coating of a prepared pressure-sensitive adhesive on a PET substrate and UV curing has excellent permanent adhesion, and has small high temperature increase.

Description

technical field [0001] The invention belongs to the technical field of adhesive tapes, in particular to a high temperature resistant UV adhesive tape. Background technique [0002] UV adhesive tape is widely used in wafer cutting, glass thinning and other fields. It can be firmly attached to materials such as silicon wafers, glass and stainless steel plates, and can effectively protect and bond transmission during cutting and etching processes. Function: After a short time of UV irradiation, the adhesion of UV adhesive tape is greatly reduced, and it is easy to tear off without residual glue. [0003] The traditional preparation method of UV viscosifying adhesive is usually realized by adding multifunctional UV resin to high-viscosity acrylic glue. This method has the characteristics of poor miscibility between resin and masterbatch, easy precipitation, and poor temperature resistance. Contents of the invention [0004] In order to solve the problems raised in the above-m...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J7/25C09J7/30C09J7/50C09J7/40
CPCC09J2203/326C09J2467/005C09J2471/006C09J7/25C09J7/30C09J7/40C09J7/50C09J2301/122C09J2301/30
Inventor 喻四海刘宇施法宽张世友刘佳周开奕赵娇娇
Owner KUNSHAN BYE MACROMOLECULE MATERIAL CO LTD
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