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A kind of epoxy composite material and preparation method thereof

A composite material and epoxy technology, which is applied in the field of thermally conductive insulating materials, can solve problems such as difficulty in meeting anti-cracking performance requirements, complex preparation procedures, etc., and achieve the effects of reducing material cost, simple preparation method and increasing filling rate.

Active Publication Date: 2022-04-12
GLOBAL ENERGY INTERCONNECTION RES INST CO LTD +3
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Therefore, the technical problem to be solved by the present invention is to overcome the defects that the epoxy resin material in the prior art is difficult to meet the anti-crack performance requirements, and the preparation process of the epoxy resin material is complicated by using fillers of various particle sizes, thereby providing a While having good thermal conductivity and insulation performance, it has strong crack resistance performance, adopts fewer types of filler particle sizes, and is an epoxy composite material with simple preparation process and its preparation method.

Method used

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  • A kind of epoxy composite material and preparation method thereof

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Embodiment 1

[0028] This embodiment provides an epoxy composite material, the raw materials include epoxy resin binder, inorganic filler, curing agent and fiber fabric; wherein the epoxy resin binder is bisphenol A epoxy resin, and the inorganic filler is boron nitride , the curing agent is phthalic anhydride, and the fiber fabric is aramid fiber fabric. The inorganic filler is composed of two kinds of boron nitride fillers with different particle sizes. The ratio of the average particle size of the large particle size filler to the small particle size filler is 1:0.4, and the average particle size of the large particle size filler is 250 μm. . In terms of volume percentage, the inorganic fillers accounted for 30% of the epoxy composite material, wherein the filler with large particle size accounted for 16.3% of the epoxy composite material, and the filler with small particle size accounted for 13.7% of the epoxy composite material.

[0029] This embodiment also provides one or more prepa...

Embodiment 2

[0031] This embodiment provides an epoxy composite material, the raw materials include epoxy resin binder, inorganic filler, curing agent and fiber fabric; wherein the epoxy resin binder is hydrogenated bisphenol A epoxy resin, and the inorganic filler is boron nitride , silicon nitride and silicon oxide in a mass ratio of 1:1:2, the curing agent is hexahydrophthalic anhydride, and the fiber fabric is a mixed fabric of aramid fiber and polyimide fiber. The inorganic filler is composed of two kinds of fillers with different particle sizes. The ratio of the average particle size of the large particle size filler to the small particle size filler is 1:0.412, and the average particle size of the large particle size filler is 18 μm. In terms of volume percentage, inorganic fillers account for 40% of the epoxy composite material, wherein the filler with large particle size accounts for 22.5% of the epoxy composite material, and the filler with small particle size accounts for 17.5% o...

Embodiment 3

[0034] This embodiment provides an epoxy composite material, the raw materials include epoxy resin binder, inorganic filler, curing agent and fiber fabric; wherein the epoxy resin binder is bisphenol F epoxy resin, and the inorganic filler is boron nitride, A mixture of aluminum nitride and silicon nitride in a mass ratio of 3:5:1, the curing agent is methyltetrahydrophthalic anhydride, and the fiber fabric is a mixed fabric of glass fiber and basalt fiber. The inorganic filler is composed of two kinds of fillers with different particle sizes. The ratio of the average particle size of the filler with a large particle size to that of the filler with a small particle size is 1:0.37, and the average particle size of the filler with a large particle size is 10 μm. In terms of volume percentage, inorganic fillers account for 37% of the epoxy composite material, among which, the filler with large particle size accounts for 20.6% of the epoxy composite material, and the filler with sm...

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Abstract

The invention provides an epoxy composite material and a preparation method thereof. The raw materials of the epoxy composite material include an epoxy resin base material, an inorganic filler, a curing agent and a fiber fabric; the inorganic filler consists of two fillers with different particle sizes Composition, the ratio of the average particle diameter of the two fillers is 1:0.37-0.45, wherein, the average particle diameter of the filler with the large particle diameter is not less than 10 μm; In terms of the volume of the filler, among the two fillers, the filler with the large particle diameter Wherein, V is the volume percentage of the inorganic filler in the epoxy composite material, and the above epoxy composite material can be effective without affecting the thermal conductivity and insulation performance by adding fiber fabrics. Improve the mechanical properties of the epoxy composite material, especially the anti-cracking performance; by using two kinds of inorganic fillers with different particle sizes, compared with the fillers with three different particle sizes, the preparation process can be simplified and the operation is simple.

Description

technical field [0001] The invention relates to the technical field of thermally conductive insulating materials, in particular to an epoxy composite material and a preparation method thereof. Background technique [0002] With the widespread access of DC power sources such as distributed power sources, new energy storage devices, fuel cells, and microgrids, as well as more and more applications of DC loads such as electric vehicles, data centers, computers, and urban rail transit, traditional power distribution networks are required. At the same time, it has the ability of AC and DC power supply and AC and DC load power supply; on the other hand, the promotion of distributed power generation technology makes the traditional power distribution system expand the function of power generation from a single power supply form, resulting in energy from traditional power generation. The unidirectional flow of source, grid and load, and the development of bidirectional flow requires...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L63/00C08L63/04C08L77/10C08L79/08C08L67/00C08K13/04C08K3/38C08K3/28C08K3/34C08K7/00C08K7/14C08K7/10
CPCC08L63/00C08L63/04C08K13/04C08K3/38C08K3/28C08K3/34C08K7/00C08K7/14C08K7/10C08K2201/003C08L2205/16C08K2003/385C08K2201/014C08L2205/03C08K2003/282C08L77/10C08L79/08C08L67/00
Inventor 陈赟张翀杨威张卓颜丙越尹立史晓宁邢照亮陈新边凯乔光尧靳艳娇苏冰
Owner GLOBAL ENERGY INTERCONNECTION RES INST CO LTD
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