A chemical pretreatment method for organic waste gas containing styrene components
A technology of organic waste gas and styrene, applied in chemical instruments and methods, separation methods, gas treatment, etc., can solve problems such as hidden dangers, pipeline and device blockage safety, etc.
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Embodiment 1
[0031] Specific steps include:
[0032] The first step, the 13X molecular sieve produced by the purchased commercialized Transung company is mixed with the phosphoric acid aqueous solution, extruded on the twin-screw extruder, and the concentration of the phosphoric acid aqueous solution used is 0.15mol / L;
[0033] The second step is to place the formed 13X molecular sieve to dry naturally at room temperature for 12 hours, and then place it in an oven and dry it at 120°C for 12 hours;
[0034] The third step, prepare a certain concentration of titanium chloride solution, the concentration is 0.35mol / L;
[0035] In the fourth step, the dried 13X molecular sieve is placed in the above titanium chloride solution, and electromagnetically stirred for 2 hours, taken out and calcined at 450° C. for 6 hours to obtain the modified 13X molecular sieve.
Embodiment 2
[0037] Specific steps include:
[0038] The first step, the 13X molecular sieve produced by the purchased commercial Transung company is mixed with the phosphoric acid aqueous solution, extruded on the twin-screw extruder, and the concentration of the phosphoric acid aqueous solution used is 0.30mol / L;
[0039] The second step is to place the formed 13X molecular sieve to dry naturally at room temperature for 12 hours, and then place it in an oven to dry at 150°C for 8 hours;
[0040] The third step, prepare a certain concentration of ferric chloride solution, the concentration is 0.40mol / L;
[0041] In the fourth step, the dried 13X molecular sieve is placed in the above titanium chloride solution, and electromagnetically stirred for 1 hour, taken out and calcined at 350° C. for 10 hours to obtain the modified 13X molecular sieve.
Embodiment 3
[0043] The first step, the 13X molecular sieve produced by the purchased commercial Transung company is mixed with the phosphoric acid aqueous solution, extruded on the twin-screw extruder, and the concentration of the phosphoric acid aqueous solution used is 0.7mol / L;
[0044] The second step is to place the formed 13X molecular sieve to dry naturally at room temperature for 12h, and then place it in an oven and dry it at 110°C for 6h;
[0045] The third step, prepare a certain concentration of zirconium chloride solution, the concentration is 0.45mol / L;
[0046] In the fourth step, the dried 13X molecular sieve is placed in the above-mentioned zirconium chloride solution, and electromagnetically stirred for 6 hours, taken out and calcined at 600° C. for 2 hours to obtain the modified 13X molecular sieve.
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