Rare earth permanent magnet material, raw material composition, preparation method, application and motor
A technology of raw material composition and permanent magnet material, which can be used in the manufacture of magnetic materials, magnetic objects, inductors/transformers/magnets, etc., which can solve the problems of Br and Hcj being difficult to achieve synchronous promotion.
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Embodiment 1
[0143] The preparation method of R-T-B series sintered magnet is as follows:
[0144] (1) Melting process: according to the formula shown in Example 1 in Table 1, get the prepared raw materials and put them into a crucible made of alumina, and put them in a high-frequency vacuum induction melting furnace at 5 × 10 -2 Vacuum melting is carried out at a temperature below 1500°C in a vacuum of Pa.
[0145] (2) Casting process: after vacuum smelting, Ar gas is passed into the smelting furnace to make the air pressure reach 55,000 Pa, and then casting is carried out at 10 2 ℃ / sec-10 4 °C / sec cooling rate to obtain quenched alloy.
[0146] (3) Hydrogen crushing process: Vacuumize the hydrogen crushing furnace where the quenched alloy is placed at room temperature, and then pass hydrogen gas with a purity of 99.9% into the hydrogen crushing furnace to maintain the hydrogen pressure at 0.15 MPa. After fully absorbing hydrogen, Heat up while evacuating to fully dehydrogenate, then c...
Embodiment 2-8、 comparative example 1-9
[0157] According to the formula shown in Table 1, the R-T-B series sintered magnets corresponding to Examples 2-8 and Comparative Examples 1-9 were obtained, wherein the preparation techniques of Examples 2-4, Comparative Examples 1-3 and Comparative Examples 6-9 were the same as Example 1.
[0158] The preparation processes of Examples 5-8 and Comparative Examples 4-5 are the same as Example 1 except for the following differences: grain boundary diffusion treatment process: the sintered body is processed into a magnet with a diameter of 20mm and a thickness of 5mm, and the thickness direction is the orientation direction of the magnetic field. After the surface is cleaned, the diffusion material containing Tb metal is sprayed and coated on the magnet, and the coated magnet is dried. In a high-purity Ar gas atmosphere, the magnet with Tb element attached to the surface is Diffusion heat treatment at a temperature of 850°C for 24 hours. After processing, cool to room temperatu...
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