Preparation method of environmentally-friendly cellulose sponge material
A cellulose sponge, an environmentally friendly technology, applied in the field of cellulose, can solve problems such as low cost, pollute the environment, corrode equipment, etc., and achieve the effect of high water absorption and good mechanical properties
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Embodiment 1
[0027] 1) Cellulose pretreatment: crush the wood pulp board into particles with a particle size of less than 50 microns, put it in an aqueous solution of sodium hydroxide for 2 hours at room temperature, filter, wash the filter cake with water, and then remove the water to obtain the pretreated fiber white;
[0028] 2) Preparation of cellulose solution: Dissolve sodium hydroxide and thiourea in water to obtain sodium hydroxide / thiourea solution (100mL: 2g sodium hydroxide: 2g thiourea), then put the pretreated cellulose into hydrogen Sodium oxide / thiourea solution (the weight percentage of cellulose is 6%), frozen at -5°C for 2h, and then thawed at room temperature to obtain the thawed cellulose solution;
[0029] 3) Preparation of cellulose sponge: Add 40 g of pore-forming agent sodium sulfate (with a particle size less than 5 microns) to 100 g of thawed cellulose solution and stir to obtain a mixed slurry, pour the mixed slurry into a mold for low-temperature molding for 72 ...
Embodiment 2
[0031] 1) Cellulose pretreatment: crush the wood pulp board into particles with a particle size of less than 50 microns, put it in an aqueous solution of sodium hydroxide for 2 hours at room temperature, filter, wash the filter cake with water, and then remove the water to obtain the pretreated fiber white;
[0032] 2) Preparation of cellulose solution: Dissolve sodium hydroxide and thiourea in water to obtain sodium hydroxide / thiourea solution (100mL: 2g sodium hydroxide: 2g thiourea), then put the pretreated cellulose into hydrogen Sodium oxide / thiourea solution (the weight percentage of cellulose is 10%wt), frozen at -5°C for 2h, and then thawed at room temperature to obtain the thawed cellulose solution;
[0033] 3) Preparation of cellulose sponge: add pore-forming agent sodium sulfate (particle size less than 5 microns) to the thawed cellulose solution and stir to obtain a mixed slurry, pour the mixed slurry into a mold for low-temperature molding for 72 hours; low-temper...
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