A polymethacrylimide foam with low smoke, low toxicity and high flame retardancy
A polymethacrylimide, high flame retardant technology, used in the field of foam material preparation, can solve the problems of reduced strength, poor temperature resistance, high toxicity and other problems of PMI foam materials, and achieves excellent mechanical properties and low smoke. Density and smoke toxicity, excellent flame retardant properties
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0086] Take 7 parts of ammonium polyphosphate coated with PEI polymer film, soak in 12 parts of diphenylmethyl phosphonate for 24 hours, and then mix 6 parts of polymethyl methacrylate and 6 parts of iron acetoacetate, total 31 parts of flame retardant system, with 50 parts of methacrylic acid, 45 parts of methacrylonitrile, 0.5 parts of itaconic acid, 1.5 parts of isopropanol, 2.5 parts of tert-butanol, 2 parts of formamide, 0.05 parts of diphenyl peroxide Add formyl, 0.05 parts of azobisisobutyronitrile, 0.08 parts of tert-butyl peroxide 2-ethylhexanoate, 0.04 parts of tert-butyl peroxybenzoate, and 0.1 parts of magnesium methacrylate into a 3L three-necked glass flask , stirred at room temperature for 0.5h to dissolve evenly. The above solution was transferred into a closed system formed by 2 glass plates and a sealed frame. In the prepolymerization stage, polymerize in a water bath at 30°C for 144 hours, and then polymerize in a water bath at 45°C for 24 hours. The post-...
Embodiment 2
[0089] Hot soak red phosphorus in methacrylic acid for 6 hours at a temperature of 50°C to obtain passivated red phosphorus, prepare 5 parts of passivated red phosphorus, soak in organic phosphorus liquid flame retardant for 24 hours, and the organic phosphorus liquid flame retardant The agent is composed of 5 parts of dimethyl methanephosphonate, 6 parts of diphenylmethyl phosphonate, and then 5 parts of polymethyl methacrylate and 5 parts of iron acetoacetate, a total of 26 parts of flame retardant system and 50 parts Parts of methacrylic acid, 40 parts of acrylonitrile, 0.5 parts of itaconic acid, 1 part of isopropanol, 2 parts of amyl alcohol, 3 parts of formamide, 0.05 parts of lauryl peroxide, 0.05 parts of azobisisobutyronitrile, Add 0.08 parts of tert-butyl 2-ethylhexanoate, 0.06 parts of di-tert-butyl peroxide, and 0.1 parts of allyl methacrylate into a 3L three-necked glass flask in sequence, and stir at room temperature for 0.5 hours to dissolve evenly. The above so...
Embodiment 3
[0092] Hot dip ammonium polyphosphate in methacrylic acid for 6 hours at a temperature of 50°C to obtain passivated ammonium polyphosphate, prepare 7 parts of passivated ammonium polyphosphate, soak in 12 parts of diphenylmethyl phosphonate, and then Take 6 parts of polymethyl methacrylate and 6 parts of iron acetoacetate, a total of 31 parts of flame retardant system, with 50 parts of methacrylic acid, 45 parts of methacrylonitrile, 0.5 parts of itaconic acid, 1.5 parts of isopropanol, 2.5 parts of tert-butanol, 2 parts of formamide, 0.05 parts of dibenzoyl peroxide, 0.05 parts of azobisisobutyronitrile, 0.08 parts of tert-butyl peroxy 2-ethylhexanoate, 0.04 parts of tert-benzoyl peroxide Butyl ester and 0.1 part of magnesium methacrylate were sequentially added into a 3L three-necked glass flask, and stirred at room temperature for 0.5h to dissolve evenly. The above solution was transferred into a closed system formed by 2 glass plates and a sealed frame. In the prepolymeri...
PUM
Property | Measurement | Unit |
---|---|---|
particle size | aaaaa | aaaaa |
density | aaaaa | aaaaa |
compressive strength | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com