Preparation method of graphene-based hydrogel with three-dimensional network structure and photo-thermal desalted water treatment application of graphene-based hydrogel
A network structure, graphene-based technology, applied in the fields of seawater desalination, high-salt concentrated water desalination, and freshwater purification, can solve the problem of low photothermal distillation efficiency, and achieves wide source of raw materials, simple preparation method, and low energy consumption. Effect
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[0022] Specific embodiment 1: This embodiment records a method for preparing a graphene-based hydrogel with a three-dimensional network structure, and the method steps are as follows:
[0023] Step 1: Disperse the graphene oxide solution with a concentration of 10 mg / mL in deionized water ultrasonically, and configure the graphene oxide solution with uniform dispersion and no flocculation;
[0024] Step 2: Add tris(hydroxymethyl)aminomethane hydrochloride to the graphene oxide solution uniformly dispersed by ultrasonic, stir and dissolve, and the tris(hydroxymethyl)aminomethane hydrochloride maintains the pH of the solution to be weakly acidic;
[0025] Step 3: Add dopamine hydrochloride to the mixed solution of step 2, and stir to dissolve;
[0026] Step 4: The above-mentioned uniformly mixed solution is subjected to a hydrothermal reaction at a high temperature, and then subjected to post-treatment to obtain a polydopamine functionalized graphene-based hydrogel.
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[0027] Embodiment 2: The method for preparing a graphene-based hydrogel with a three-dimensional network structure described in Embodiment 1. In step 1, the mass concentration of the dispersed graphene oxide solution is 1.0-4.0 mg / mL.
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[0028] Specific Embodiment Three: In the method for preparing a graphene-based hydrogel with a three-dimensional network structure described in specific embodiment 1, in step 1, the ultrasonic dispersion time is 15-20 minutes. If the ultrasound time is too short, the flake graphene oxide cannot be completely peeled off.
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