Solvent-free silane-terminated modified polyether three-proofing paint and preparation method thereof
A silane-terminated, solvent-free technology, applied in the field of materials, can solve the problems of low bonding strength of substrates, human hazards, slow surface drying time, etc., and achieve excellent water resistance and salt spray resistance, high tensile strength , good flexibility
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[0053] The present invention provides a method for preparing the solvent-free silyl-terminated polyether conformal paint described in any one of the above technical solutions, comprising:
[0054] A) mixing and dispersing the α-terminated silyl-modified polyether resin, the γ-terminated silyl-modified polyether resin, a plasticizer, and a moisture scavenger to obtain a dispersed component;
[0055] B) mixing and stirring the dispersed components with a crosslinking agent, a heat-resistant stabilizer, an adhesion promoter and an ultraviolet absorber, and vacuum defoaming to obtain a solvent-free silyl-terminated polyether three-proof paint.
[0056] The preparation method of the solvent-free silyl-terminated polyether conformal paint provided by the present invention firstly mixes α-terminated silyl-modified polyether resin, γ-terminated silyl-modified polyether resin, plasticizer, water Cleaner mix.
[0057] The present invention does not limit the mixing equipment, which may...
Embodiment 1
[0067] 55 parts by mass of Wacker resin Wacker resin of XT 50, 35 parts by mass Add STP-E35, 3 parts by mass of hydrophobic plasticizer Mesamoll, and 1 part by mass of water scavenger to the planetary kettle for high-speed dispersion for 10 minutes, add 3 parts by mass of tetraethyl orthosilicate, 0.5 parts by mass of heat-resistant and stable Agent 1010, 2 parts by mass of adhesion promoter A-1120, 0.5 parts by mass of UV absorber 326, continue to stir for 30 minutes, turn on the vacuum, keep the vacuum degree greater than 0.1MPa, and discharge after 10 minutes of defoaming.
Embodiment 2
[0069] 55 parts by mass of Wacker resin Wacker resin of STP-E10, 35 parts by mass Add STP-E35, 3 parts by mass of hydrophobic plasticizer Mesamoll, and 1 part by mass of water scavenger to the planetary kettle for high-speed dispersion for 10 minutes, add 3 parts by mass of tetraethyl orthosilicate, 0.5 parts by mass of heat-resistant and stable Agent 1010, 2 parts by mass of adhesion promoter A-1120, 0.5 parts by mass of UV absorber 326, continue to stir for 30 minutes, turn on the vacuum, keep the vacuum degree greater than 0.1MPa, and discharge after 10 minutes of defoaming.
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