Production device and preparation technology of mixed raw material high temperature resistant capacitance film for automobile
A technology of mixing raw materials and production equipment, which is applied to the parts of fixed capacitors, fixed capacitor shells/packages, laminated capacitors, etc., can solve the problem of poor uniformity of film-forming capacitor films, and achieve high cooling molding quality , Improve high temperature resistance and stable film forming performance
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Embodiment 1
[0046] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0047] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0048] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0049] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 6:2:1 to obtain a mixed solution, and graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, continue to stir and oscillate for 45 minutes, pour the obtained solution into a crystallization kettl...
Embodiment 2
[0057] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0058] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0059] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0060] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 5:2:1 to obtain a mixed solution; graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, and continue to stir and oscillate for 45 minutes; pour the obtained solution into a crystallization kettl...
Embodiment 3
[0068] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0069] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0070] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0071] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 7:2:1 to obtain a mixed solution; graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, continue to stir and oscillate for 45 minutes; pour the obtained solution into a crystallization kettle at...
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