Bipolar plate, its preparation method and application
A bipolar plate and anodic oxidation technology, applied in the direction of final product manufacturing, sustainable manufacturing/processing, electrochemical generators, etc., can solve the problem of inability to meet the strong corrosive and harsh working environment of PEMFCs, poor mechanical strength, poor corrosion resistance, etc. question
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[0042] The method for preparing the above-mentioned bipolar plate 100 includes the following steps S110-S160:
[0043] S110 , providing a metal base 10 .
[0044] In this embodiment, the metal base 10 is titanium, titanium alloy or stainless steel.
[0045] It can be understood that the metal base 10 may be any metal base used for metal-based bipolar plates, not limited to the ones listed above.
[0046] In order to reduce the weight of the bipolar plate, thereby reducing the weight of the cell stack, in this embodiment, the thickness of the metal base 10 is 0.1 mm˜2 mm.
[0047] S120 , forming a porous metal oxide film layer 20 on the surface of the metal substrate 10 .
[0048] In this embodiment, the method for forming the porous metal oxide film layer 20 on the surface of the metal base 10 is: anodizing the metal base 10 .
[0049] Specifically, the conditions of anodic oxidation are: the metal substrate 10 is used as the anode, the graphite electrode is used as the cat...
Embodiment 1
[0091] 1) After grinding and polishing the surface of the titanium metal substrate, it is anodized to form a porous metal oxide film layer, and its surface is as follows: figure 2 As shown, the conditions of anodic oxidation are: the titanium metal substrate is used as the anode, the graphite electrode is used as the cathode, the area ratio of the cathode and the anode is about 1:8, and the electrolyte is a mixed solution of sulfuric acid and hydrochloric acid with a pH value of about 1, wherein the sulfuric acid The concentration is 350g / L, the concentration of hydrochloric acid is 50g / L; the temperature is room temperature (25°C), and the polarization current density is 3.2A / cm 2 , the time is 40min.
[0092] 2) Configure the hydroxyapatite hydrothermal reaction solution (1g / LCa(CH 3 COO) 2 ·H 2 O; 0.5g / LNaH 2 PO 4 , NaOH to adjust the pH value to 12), the above-mentioned titanium metal substrate forming a porous metal oxide film is placed in the hydrothermal reaction ...
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