Gel electrode, full-gel-state ion thermoelectric supercapacitor and preparation of full-gel-state ion thermoelectric supercapacitor
A technology for supercapacitors and electrodes, which is applied in the field of gel electrodes and all-gel ion thermoelectric supercapacitors and their preparation, can solve the problems of poor flexibility and unfriendly environment of ion thermoelectric supercapacitors, and achieve environmental friendliness and good application prospects , the effect of simple process
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Embodiment 1
[0042] (1) Disperse 50 mg of carbon nanotubes in 10 ml of ultrapure water, and sonicate for 1 hour to obtain a carbon nanotube dispersion;
[0043] (2) Add 1000 mg of acrylamide monomer, 10 mg of ammonium persulfate, and 1 mg of N,N-methylenebisacrylamide to the above carbon nanotube dispersion, and stir for 10 minutes;
[0044] (3) Transfer the above dispersion to an oven, heat and cure at 60°C for 30 minutes to obtain a CNTs / PAM hybrid gel electrode;
[0045] (4) 3.6g NaCl is dissolved in the saturated NaCl solution that 10ml ultrapure water makes;
[0046] (5) Add 1000 mg of acrylamide monomer, 10 mg of ammonium persulfate, and 1 mg of N,N-methylenebisacrylamide to the above saturated NaCl solution, and stir for 10 minutes;
[0047] (6) Transfer the above dispersion to an oven, heat and cure at a temperature of 60° C. for 30 minutes to obtain NaCl-PAM gel electrolyte;
[0048] (7) Soak the CNTs / PAM gel electrode in saturated NaCl solution for 12 hours, take it out and dry...
Embodiment 2
[0052] (1) Disperse 80 mg of carbon nanotubes in 10 ml of ultrapure water, and sonicate for 1.5 hours to obtain a carbon nanotube dispersion;
[0053] (2) Add 1500 mg of acrylamide monomer, 30 mg of ammonium persulfate, and 2 mg of N,N-methylenebisacrylamide to the above carbon nanotube dispersion, and stir for 20 minutes;
[0054] (3) Transfer the above dispersion to an oven, heat and cure at 70°C for 60 minutes to obtain a CNTs / PAM hybrid gel electrode;
[0055] (4) 3.6g NaCl is dissolved in the saturated NaCl solution that 10ml ultrapure water makes;
[0056] (5) Add 1500 mg of acrylamide monomer, 30 mg of ammonium persulfate, and 2 mg of N,N-methylenebisacrylamide to the above saturated NaCl solution, and stir for 20 minutes;
[0057] (6) Transfer the above dispersion to an oven, heat and cure at a temperature of 70° C. for 60 minutes to obtain NaCl-PAM gel electrolyte;
[0058] (7) Soak the CNTs / PAM gel electrode in saturated NaCl solution for 18 hours, take it out and ...
Embodiment 3
[0064] (1) Disperse 100mg of carbon nanotubes in 10ml of ultra-pure water, and ultrasonicate for 2 hours to obtain a carbon nanotube dispersion;
[0065] (2) Add 2000 mg of acrylamide monomer, 60 mg of ammonium persulfate, and 3 mg of N, N-methylenebisacrylamide to the above carbon nanotube dispersion, and stir for 30 minutes;
[0066] (3) Transfer the above dispersion to an oven, heat and cure at 80°C for 90 minutes to obtain a CNTs / PAM hybrid gel electrode;
[0067] (4) 3.6g NaCl is dissolved in the saturated NaCl solution that 10ml ultrapure water makes;
[0068] (5) Add 2000 mg of acrylamide monomer, 60 mg of ammonium persulfate, and 3 mg of N,N-methylenebisacrylamide to the above saturated NaCl solution, and stir for 30 minutes;
[0069] (6) Transfer the above dispersion to an oven, heat and cure at 80°C for 90 minutes to obtain NaCl-PAM gel electrolyte;
[0070] (7) Soak the CNTs / PAM gel electrode in a saturated NaCl solution for 24 hours, take it out and dry it for 30...
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