Wave-absorbing material based on recycling of agricultural and forestry wastes and preparation method thereof
A technology of agricultural and forestry wastes and wave-absorbing materials is applied in the field of wave-absorbing materials based on the reuse of agricultural and forestry wastes and their preparation, and achieves the effects of rich types, good dielectric loss capability and improved microwave absorption capability.
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Embodiment 1
[0045] This embodiment is based on the microwave-absorbing material and its preparation method for the reuse of agricultural and forestry waste, including the following steps:
[0046] (1) Preparation of raw materials: Wash and crush the purchased walnut shells through a 60-mesh sieve, wash them with water and ethanol in sequence, and dry them for later use;
[0047] (2) Ultrasonic activation pretreatment: Take 5g of the dry shell powder from the previous step, mix it with the activator potassium hydroxide at a carbon agent mass ratio of 1:1.5, add it to 75ml deionized water, and perform ultrasonic pretreatment on it for 60 minutes. Filter and dry at 60°C;
[0048] (3) Stage heating carbonization treatment: Take an appropriate amount of the pretreated material in the previous step and put it into a tube furnace, and carry out carbonization reaction treatment in an argon atmosphere. The carbonization process adopts a staged temperature program. Stage heating and carbonization ...
Embodiment 2
[0051] This embodiment is based on the microwave-absorbing material and its preparation method for the reuse of agricultural and forestry waste, including the following steps:
[0052] (1) Preparation of raw materials: Wash and crush the purchased walnut shells through a 60-mesh sieve, wash them with water and ethanol in sequence, and dry them for later use;
[0053] (2) Ultrasonic activation pretreatment: Take 5g of the dry shell powder from the previous step, mix it with the activator potassium hydroxide at a carbon agent mass ratio of 1:1.5, add it to 75ml deionized water, and perform ultrasonic pretreatment on it for 60 minutes. Filter and dry at 60°C;
[0054] (3) Stage heating carbonization treatment: Take an appropriate amount of the pretreated material in the previous step and put it into a tube furnace, and carry out carbonization reaction treatment in an argon atmosphere. The carbonization process adopts a staged temperature program. Stage heating and carbonization ...
Embodiment 3
[0057] This embodiment is based on the microwave-absorbing material and its preparation method for the reuse of agricultural and forestry waste, including the following steps:
[0058] (1) Preparation of raw materials: Wash and pulverize the purchased radix sorbifolia husk through a 60-mesh sieve, wash with water and ethanol in sequence, and dry for later use;
[0059] (2) Ultrasonic activation pretreatment: Take 5g of the dried shell powder from the previous step, mix them with the activator potassium hydroxide and sodium hydroxide according to the carbon agent mass ratio of 1:1.5, add them to 75ml of deionized water, and perform ultrasonic pretreatment on it After 60 minutes, suction filter and dry at 60°C;
[0060] (3) Stage heating carbonization treatment: Take an appropriate amount of the pretreated material in the previous step and put it into a tube furnace, and carry out carbonization reaction treatment in an argon atmosphere. The carbonization process adopts a staged ...
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