Imidazoline derivatives as well as synthesis method and application thereof
A technology of imidazoline derivatives and synthesis methods, applied in chemical instruments and methods, water/sludge/sewage treatment, organic chemistry, etc., can solve the problem of increased concentration of corrosion inhibitors and difficulty in compatibility with various environmental conditions , increase the cost of oilfield sewage treatment and other issues
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[0040] Such as figure 1 As shown, the synthetic method of the imidazoline derivative provided by the embodiment of the present invention comprises the following steps:
[0041] S101: Synthesis of imidazoline intermediates. Heat oleic acid to 160°C in a reaction vessel, add triethylenetetramine and xylene at a molar ratio of 1:1.2:1.2, and perform amidation reaction for three hours; raise the temperature to 230°C, and perform dehydration and cyclization for three hours (using a few minutes during the period) The water device separates the xylene and water), and cools to room temperature to obtain the imidazoline intermediate.
[0042] S102: Synthesis of imidazoline derivatives. Add the imidazoline intermediate to the reaction vessel and raise the temperature to 95°C, add acetophenone, drop hydrochloric acid into the formaldehyde, add the intermediate and acetophenone to the reaction system; react at 95°C for 5 hours to obtain Dark reddish brown viscous imidazoline derivativ...
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