Compound, display panel and display device
A display panel and compound technology, which is applied in the fields of compounds, display panels and display devices, can solve the problems of affecting OLED luminous quantum efficiency, reducing component efficiency and thermal stability, and reducing exciton formation efficiency, so as to achieve suppression of electron transport performance and Reduced exciton formation efficiency, enhanced electron injection and transport capabilities, and effects of high exciton utilization
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[0130] Example 1: Synthesis of compound H-25
[0131] (One)
[0132] Under a nitrogen atmosphere, add re-2 (5 mmol) to 100 mL of anhydrous THF, stir at -78°C for 10 min, wait for the reaction solution to cool, and add 1.6M n-BuLi (5 mmol) dropwise until the addition is complete. React at -78℃ for 2h; dissolve re-1 (5mmol) in 50mL anhydrous THF solution, then add it dropwise to the low-temperature reaction solution with a syringe. When the addition is over, continue the reaction at low temperature for 1h, then warm to room temperature for reaction 6h. After the reaction is over, add a small amount of water to quench, add water and dichloromethane for extraction, collect the organic phase and dry with anhydrous sodium sulfate, collect the filtrate by suction and spin off the solvent to obtain a crude product.
[0133] The above crude product was added to 80 mL of acetic acid under nitrogen conditions, stirred and heated, and reacted at 120° C. for 2 h, and then 5 mL of hydrochloric ...
Example Embodiment
[0139] Example 2: Synthesis of compound H-50
[0140] (two)
[0141] The preparation method is similar to that of Example 1, except that re-3 in step (2) of Example 1 is replaced with an equimolar amount of re-4 to finally obtain the target compound H-50 (yield 78%).
[0142] LC-MS: m / z: calculated value: C58H36N4OS: 837.00, measured value: 836.79.
[0143] Elemental analysis results of the compound: calculated value: C58H36N4OS (%): C 83.23, H 4.34, N 6.69; test value: C 83.24, H 4.35, N 6.70.
Example Embodiment
[0144] Example 3: Synthesis of compound H-53
[0145] (two)
[0146] The preparation method is similar to that of Example 1, except that re-3 in step (2) of Example 1 is replaced with an equimolar amount of re-5 to finally obtain the target compound H-53 (yield 75%).
[0147] LC-MS: m / z: calculated value: C56H34N6OS: 838.97, measured value: 838.61.
[0148] Elemental analysis results of the compound: calculated value: C56H34N6OS (%): C 80.17, H 4.08, N 10.02; test value: C 80.18, H 4.07, N 10.04.
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