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Acrylic resin and its preparation method
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A technology of acrylic resin and pentene, applied in the direction of coating, can solve the problems to be improved, the boiling water resistance and hydrophobicity of acrylic resin are not ideal, and achieve good high and low temperature resistance, boiling water resistance and excellent hydrophobicity. Effect
Active Publication Date: 2022-03-04
上海元邦化工制造有限公司
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Problems solved by technology
[0004] In the prior art, the boiling water resistance and hydrophobic properties of acrylic resins are not ideal and need to be improved
Method used
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Embodiment 1
[0039] A kind of acrylic resin, adopts following method to prepare:
[0040] (1) 110 grams of ethylene glycol monobutyl ether is heated to 110 ° C;
[0041] (2) Mix 100 grams of complex monomers, 3.5 grams of di-tert-butyl peroxide, and 0.4 grams of 2,4-diphenyl-4-methyl-1-pentene, and add the above-mentioned ethylene glycol monobutylene dropwise. In ether, the dropping time is 3 hours, and the temperature is kept at 110°C for 3 hours;
[0042] (3) The solvent was evaporated under reduced pressure, and dried at 90° C. for 3 hours to obtain the acrylic resin.
[0043] The composite monomer is formed by mixing monomer A, monomer B, monomer C, monomer D and monomer E. The mass ratio of monomer A, monomer B, monomer C, monomer D and monomer E is 35:35:10:10:10.
Embodiment 2
[0045] A kind of acrylic resin, adopts following method to prepare:
[0046] (1) 110 grams of ethylene glycol monobutyl ether is heated to 110 ° C;
[0047] (2) Mix 100 grams of complex monomers, 3.5 grams of di-tert-butyl peroxide, and 0.4 grams of 2,4-diphenyl-4-methyl-1-pentene, and add the above-mentioned ethylene glycol monobutylene dropwise. In ether, the dropping time is 3 hours, and the temperature is kept at 110°C for 3 hours;
[0048] (3) The solvent was evaporated under reduced pressure, and dried at 90° C. for 3 hours to obtain the acrylic resin.
[0049] The composite monomer is formed by mixing monomer B, monomer C, monomer D and monomer E. The mass ratio of monomer B, monomer C, monomer D and monomer E is 70:10:10:10.
Embodiment 3
[0051] A kind of acrylic resin, adopts following method to prepare:
[0052] (1) 110 grams of ethylene glycol monobutyl ether is heated to 110 ° C;
[0053] (2) Mix 100 grams of complex monomers, 3.5 grams of di-tert-butyl peroxide, and 0.4 grams of 2,4-diphenyl-4-methyl-1-pentene, and add the above-mentioned ethylene glycol monobutylene dropwise. In ether, the dropping time is 3 hours, and the temperature is kept at 110°C for 3 hours;
[0054] (3) The solvent was evaporated under reduced pressure, and dried at 90° C. for 3 hours to obtain the acrylic resin.
[0055] The composite monomer is formed by mixing monomer A, monomer C, monomer D and monomer E. The mass ratio of monomer A, monomer C, monomer D and monomer E is 70:10:10:10.
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
technical field [0001] The invention relates to an acrylic resin and a preparation method thereof. Background technique [0002] Acrylic resin is a commonly used chemical material, mainly used as paint and used in textile printing and dyeing. Acrylic resins are copolymerized from acrylates or methacrylates and other ethylenic monomers. The main raw materials of acrylic resin are: monomer, initiator, solvent and chain transfer agent, any adjustment of any raw material will affect the performance of the product. [0003] By selecting different acrylic resins, different pigments, additives, solvents and crosslinking agents. It can synthesize acrylic paints with various types, performances and applications. [0004] In the prior art, the boiling water resistance and hydrophobicity of the acrylic resin are not ideal and need to be improved. Contents of the invention [0005] Aiming at the deficiencies in the prior art, the technical problem to be solved by the present inven...
Claims
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