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Method for improving response of optical excitation flexible substrate gas sensor at room temperature

A gas sensor, flexible substrate technology, applied in instruments, scientific instruments, measuring devices, etc., can solve the problems of underutilization of sensitive materials, huge pressure in the preparation of sensitive materials, etc., and is beneficial to large-scale promotion and utilization, The effect of improving photogenerated charge separation efficiency and improving gas sensing performance

Active Publication Date: 2020-11-10
SOUTHWEST UNIVERSITY FOR NATIONALITIES +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In the past, the sensitivity of sensors for detecting target gases was almost without exception, which caused great pressure in the preparation of sensitive materials. Even under the condition of light excitation, the sensitive materials of flexible gas sensors were not fully exposed to light, that is to say, the sensitive materials themselves were not exposed to light. is fully utilized, which is also a common problem in the field

Method used

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  • Method for improving response of optical excitation flexible substrate gas sensor at room temperature
  • Method for improving response of optical excitation flexible substrate gas sensor at room temperature
  • Method for improving response of optical excitation flexible substrate gas sensor at room temperature

Examples

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Comparison scheme
Effect test

Embodiment 1

[0033] Such as Figure 1-5 As shown, a method for improving the response of a light-excited flexible substrate gas sensor at room temperature includes the following steps:

[0034] (1) The polyimide flexible base layer 4 with a thickness of 150 μm is ultrasonically cleaned with acetone, the power is 40 W, and the ultrasonic time is 5 min to remove oil stains on the surface. Rinse with deionized water repeatedly until the deionized water remains evenly on the surface, then rinse it in analytical pure ethanol, take it out and blow dry.

[0035] (2) Put the substrate in step (1) into the coating machine while filling it with argon gas, and use the electron emission electrons from the vacuum chamber of the coating machine to make the argon gas store and bombard the surface of the substrate to improve the cleanliness of the substrate. The flow rate of argon is 100 sccm, and the electrode voltage of the coater is 50W.

[0036] (3) Prepare a metal aluminum film on the surface of the substr...

Embodiment 2

[0043] Such as Figure 1-4 As shown, based on Example 1, a method for improving the response of a light-excited flexible substrate gas sensor at room temperature includes the following steps:

[0044] (1) The polyimide flexible base layer 4 with a thickness of 150 μm is ultrasonically cleaned with acetone, the power is 30 W, and the ultrasonic time is 10 min to remove oil stains on the surface. Rinse with deionized water repeatedly until the deionized water remains evenly on the surface, then rinse it in analytical pure ethanol, take it out and blow dry.

[0045] (2) Put the substrate in step (1) into the coating machine while filling it with argon gas, and use the electron emission electrons from the vacuum chamber of the coating machine to make the argon gas store and bombard the surface of the substrate to improve the cleanliness of the substrate. The flow of argon is 100 sccm, and the electrode voltage of the coater is 40W.

[0046] (3) Prepare a metal platinum film on the surf...

Embodiment 3

[0050] Such as Figure 1-4 As shown, based on Example 1, a method for improving the response of a light-excited flexible substrate gas sensor at room temperature includes the following steps:

[0051] (1) The polyimide flexible base layer 4 with a thickness of 150 μm is ultrasonically cleaned with acetone, the power is 30 W, and the ultrasonic time is 5 min to remove oil stains on the surface. Rinse with deionized water repeatedly until the deionized water remains evenly on the surface, then rinse it in analytical pure ethanol, take it out and blow dry.

[0052] (2) Put the substrate in step (1) into the coating machine while filling it with argon gas, and use the electron emission electrons from the vacuum chamber of the coating machine to make the argon gas store and bombard the surface of the substrate to improve the cleanliness of the substrate. The argon flow rate is 80 sccm, and the electrode voltage of the coater is 40W.

[0053] (3) Prepare a metal zinc film on the surface ...

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Abstract

The invention discloses a method for improving response of an optical excitation flexible substrate gas sensitive sensor at room temperature, belongs to the field of gas sensing, particularly relatesto the field of preparation of flexible gas sensitive sensors, and aims to overcome the defect that a sensitive material is not fully utilized in the past, and the method comprises the following steps: (1) cleaning and blow-drying a flexible substrate layer; (2) putting the flexible substrate layer into a coating machine, and ionizing argon and bombarding the surface of the flexible substrate layer by utilizing electric emission electrons; (3) preparing a flexible substrate layer by using a magnetron sputtering instrument to prepare a metal film reflecting layer; and (4) repeatedly cleaning the flexible substrate layer plated with the metal film reflecting layer with deionized water and drying for later use, and sequentially preparing an interdigital electrode layer and a gas sensitive film layer on one side, far away from the metal film reflecting layer, of the flexible substrate layer. According to the method, the upper surface and the lower surface of the sensitive material can be in full contact with light, the surface photo-induced electron concentration of the gas sensitive material can be effectively increased, and the photo-induced charge separation efficiency is improved,so that the gas sensitive performance is improved.

Description

Technical field [0001] A method for improving the response of a light-excited flexible substrate gas sensor under room temperature conditions. The invention belongs to the technical field of gas sensing, and specifically relates to the technical field of flexible gas sensor preparation. Background technique [0002] Due to the unique performance and potential application and market value of flexible gas sensors, many research institutions at home and abroad have carried out research on flexible gas sensors. The flexible substrate in the flexible gas sensor generally includes organic materials such as polyvinyl alcohol (PVA), polyimide (PI), polyester (PET), polyethersulfone (PES), acid-free paper, textile materials, and copper Metal materials such as foil and stainless steel foil; their gas-sensitive materials can be divided into two categories: single material and composite material. Although flexible gas sensors based on different gas-sensitive materials have made some progres...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/12G01N27/04
CPCG01N27/122G01N27/125G01N27/045Y02A50/20
Inventor 袁欢刘文钰徐明隆小芹吴国畅
Owner SOUTHWEST UNIVERSITY FOR NATIONALITIES