Synthesis process of degradable biopolymer material

A biopolymer and synthesis process technology, applied in the field of synthesis of degradable biopolymer materials, can solve the problems of long time consumption, complex synthesis process, difficult long-term transportation, etc., to achieve improved coalescence performance, simple process synthesis, Prolonged long-acting effect

Inactive Publication Date: 2021-01-15
HUNAN UNIV OF ARTS & SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the deficiencies of the prior art, the present invention provides a synthesis process of degradable biopolymer materials, which solves the problem that the synthesis process of the existing degradable biopolymer materials proposed in the above-mentioned background technology is complex and takes a long time , the storage time is short, it is difficult to transport for a long time, and it is not easy to form

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment example 1

[0026] The invention provides a technical solution: a synthesis process of degradable biopolymer materials, which is composed of the following components in parts by weight: 40 parts of degradable polymers produced by microorganisms, 30 parts of epoxy resin, and unitary monophthalamide resin 10 parts, 15 parts of lactating acid, 10 parts of lactic acid, 6 parts of talcum powder, 4 parts of coalescence aid, 3 parts of catalyst, 1 part of modifier, 2 parts of thickener, 1 part of compatibilizer, coupling agent 3 parts, 3 parts of toughening agent, 5 parts of fungicide.

[0027] Microbial production of degradable polymers consists of one or more of microbial polyesters, polylactic acid, microbial polysaccharides, copolymers of 3-hydroxybutyrate and 3-hydroxyvalerate, and the film-forming aid is composed of propylene glycol butyrate At least one of ether and propylene glycol methyl ether acetate.

[0028] The catalyst is a homogeneous catalyst with one or two of acid, alkali, sol...

Embodiment example 2

[0043] A synthesis process for degradable biopolymer materials, which is composed of the following ingredients in parts by weight: 50 parts of degradable polymers produced by microorganisms, 40 parts of epoxy resin, 20 parts of monophthalamide resin, and 25 parts of polyacrylic acid , 20 parts of lactic acid, 10 parts of talcum powder, 8 parts of coalescent, 5 parts of catalyst, 3 parts of modifier, 5 parts of thickener, 2 parts of compatibilizer, 5 parts of coupling agent, 3 parts of toughening agent , 5 parts of fungicides.

[0044] Microbial production of degradable polymers consists of one or more of microbial polyesters, polylactic acid, microbial polysaccharides, copolymers of 3-hydroxybutyrate and 3-hydroxyvalerate, and the film-forming aid is composed of propylene glycol butyrate At least one of ether and propylene glycol methyl ether acetate.

[0045] The catalyst is a homogeneous catalyst with one or two of acid, alkali, soluble transition metal compound and peroxid...

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Abstract

The invention discloses a synthesis process of a degradable biopolymer material, and relates to the technical field of synthesis of degradable biopolymer materials, in particular to a synthesis process of a degradable biopolymer material. The degradable biopolymer material is prepared from the following components in parts by weight: 40-50 parts of degradable macromolecules, 30-40 parts of epoxy resin, 10-20 parts of unitary phthalamide resin, 15-25 parts of lactide, 10-20 parts of lactic acid, 6-10 parts of talcum powder, 4-8 parts of a coalescing agent, 3-5 parts of a catalyst, 1-3 parts ofa modifier, 2-5 parts of a thickener, 1-2 parts of a compatilizer, 3-5 parts of a coupling agent, 2-3 parts of a flexibilizer and 1-5 parts of a bactericide. According to the synthesis process of thedegradable biopolymer material, the coalescing agent can promote plastic flow and elastic deformation of a polymer compound, improve coalescence performance, form a film in a wide construction temperature range, the catalyst can effectively promote the mixing efficiency of raw materials, and the thickener can effectively increase the mixing concentration of the raw materials; and the raw materialmixing uniformity is improved.

Description

technical field [0001] The invention relates to the technical field of synthesis of degradable biopolymer materials, in particular to a synthesis process of degradable biopolymer materials. Background technique [0002] People have deeply studied the biodegradability of different biodegradable polymer materials, and found that it has a great relationship with its structure, including chemical structure, physical structure, surface structure and so on. The chemical structure of polymer materials directly affects the strength of biodegradability, in general: aliphatic ester bond, peptide bond > carbamate > aliphatic ether bond > methylene. When the solid state structure of the same material is different, the degradation speed of different aggregation states is in the following order: rubber state > glass state > crystalline state. Generally, polymer materials with high polarity can adhere to the enzyme phase and have a good affinity. The way microorganisms adhe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L67/00C08L67/04C08L5/00C08L63/00C08K13/02C08K3/34C08K5/05
CPCC08L67/00C08L67/04C08L5/00C08L2201/06C08L63/00C08K13/02C08K3/34C08K5/05
Inventor 王菲菲黄雨荷黎敏戴双媛
Owner HUNAN UNIV OF ARTS & SCI
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