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Cleaning solution for removing water spots on surface of metallographic specimen and using method thereof

A metallographic sample and cleaning solution technology, which is applied in the preparation of test samples, non-surface active detergent compositions, inorganic non-surface active cleaning compositions, etc., can solve the problem of affecting photographic effect, low work efficiency, sample Surface rust and other problems, to achieve the effect of reducing the number of repeated preparations, easy configuration and storage, and simple steps of use

Inactive Publication Date: 2021-02-02
XIAN THERMAL POWER RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For inlaid metallographic samples, as well as samples with cracks or coatings, since moisture, polishing paste, and debris generated during the sample preparation process are likely to remain in the gaps or holes, cleaning with absolute ethanol and drying with hot air cannot Remove stains in gaps or holes. Affected by capillarity, residual moisture and impurities will gradually seep out of the gaps during the photographing process, and stains will form near the gaps of the sample, affecting the photographic effect; for materials with weak corrosion resistance , the seepage of water stains may cause the surface of the sample to rust, causing misjudgment of the metallographic structure of the material
At present, the sample cleaning methods are mostly repeated cleaning and drying, and try to complete the shooting before the water stain seeps out. Usually, a sample needs to be repeated many times to complete the observation and analysis. The work intensity is high and the work efficiency is low.

Method used

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  • Cleaning solution for removing water spots on surface of metallographic specimen and using method thereof
  • Cleaning solution for removing water spots on surface of metallographic specimen and using method thereof
  • Cleaning solution for removing water spots on surface of metallographic specimen and using method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0023] A cleaning solution for removing water stains on the surface of a metallographic sample and a method of use thereof provided by the invention are composed of the following components according to the weight ratio: deionized water 100mL, anhydrous sodium carbonate 3g, EDTA (ethylenediamine Tetraacetic acid) 3g.

[0024] Configuration and cleaning steps:

[0025] (1), first add 3g of anhydrous sodium carbonate into 100mL of deionized water and stir continuously to fully dissolve, then add 3g of EDTA (ethylenediaminetetraacetic acid) powder into the sodium carbonate solution and continuously stir to fully dissolve;

[0026] (2) Immerse the sample in the solution and put it into an ultrasonic cleaning machine for cleaning for about 10 minutes;

[0027] (3) Spray absolute alcohol on the surface of the sample after ultrasonic cleaning and dry it, then metallographic observation and photography can be carried out.

[0028] Cleaning effect: Since moisture is easy to remain in...

Embodiment 2

[0030] A cleaning solution for removing water stains on the surface of a metallographic sample and a method of use thereof provided by the invention are composed of the following components according to the weight ratio: deionized water 100mL, anhydrous sodium carbonate 6g, EDTA (ethylenediamine Tetraacetic acid) 3g.

[0031] Configuration and cleaning steps:

[0032] (1), first add 6g of anhydrous sodium carbonate into 100mL of deionized water and stir continuously to fully dissolve, then add 3g of EDTA (ethylenediaminetetraacetic acid) powder into the sodium carbonate solution and continuously stir to fully dissolve;

[0033] (2) Immerse the sample in the solution and put it into an ultrasonic cleaning machine for cleaning for about 10 minutes;

[0034] (3) Spray absolute alcohol on the surface of the sample after ultrasonic cleaning and dry it, then metallographic observation and photography can be carried out.

[0035] Cleaning effect: Since moisture is easy to remain in...

Embodiment 3

[0037] A cleaning solution for removing water stains on the surface of a metallographic sample and a method of use thereof provided by the invention are composed of the following components according to the weight ratio: deionized water 100mL, anhydrous sodium carbonate 30g, EDTA (ethylenediamine Tetraacetic acid) 30g.

[0038] Configuration and cleaning steps:

[0039] (1), first add 30g of anhydrous sodium carbonate into 100mL of deionized water and stir continuously to fully dissolve, then add 30g of EDTA (ethylenediaminetetraacetic acid) powder into the sodium carbonate solution and continuously stir to fully dissolve;

[0040] (2) Immerse the sample in the solution and put it into an ultrasonic cleaning machine for cleaning for about 10 minutes;

[0041] (3) Spray absolute alcohol on the surface of the sample after ultrasonic cleaning and dry it, then metallographic observation and photography can be carried out.

[0042] Cleaning effect: Since moisture is easy to remai...

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Abstract

The invention discloses a cleaning solution for removing water spots on the surface of a metallographic specimen and a use method thereof, and particularly relates to the field of metallographic specimen preparation and metal surface treatment, and the formula comprises the following raw materials by weight: 100g of deionized water, 3-30g of anhydrous sodium carbonate and 3-30g of EDTA (ethylenediamine tetraacetic acid) at room temperature, wherein the weight ratio of anhydrous sodium carbonate to EDTA is about 1:1-2:1. The method can effectively solve the problem of water stain residue causedby water seepage or incomplete cleaning on the surfaces of metallographic specimens and other specimens with high requirements on the cleanliness of the alloy surface, can make a metallographic observation surface bright and clean, and effectively identifies the grain boundary, precipitated phase and crack tip morphology.

Description

technical field [0001] The invention belongs to the field of metallographic sample preparation and metal surface treatment, and specifically relates to a cleaning solution for removing water stains on the surface of metallographic samples and a method for using the same, and is especially suitable for metallographic samples that require relatively high cleanliness on the surface of alloys. High sample water spot cleaning. Background technique [0002] Metallographic testing methods are widely used in material quality testing, and are also one of the must-test items for component failure analysis. Although the method of metallographic detection is simple and widely used, in order to obtain ideal metallographic structure photos, the requirements for the surface state of the metal sample are extremely high, and it is necessary to make the sample as bright as a mirror through continuous grinding and polishing; Clean and dry the remaining polishing paste on the surface with abso...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11D7/12C11D7/32C11D7/60G01N1/28G01N1/34G01N21/84
CPCC11D7/12C11D7/3245G01N1/28G01N1/34G01N21/84
Inventor 李季侯淑芳宁娜唐丽英周荣灿李江王博涵
Owner XIAN THERMAL POWER RES INST CO LTD
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