A kind of preparation method of building tile grout
A technology of caulking agent and ceramic tiles, which is applied in the field of building materials, can solve the problems of ceramic tile caulking agents such as reduced pan-alkali resistance, unfavorable industrialization, and reduced strength, and achieves the effects of reducing pan-alkali phenomenon, reducing content, and improving compactness
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Embodiment 1
[0025] A preparation method for building tile grout, comprising the following steps:
[0026] (1) Dissolve polyvinyl alcohol in an aqueous ethanol solution with a mass fraction of 20% at 90°C, and then add water-soluble resin liquid to obtain polyvinyl alcohol glue;
[0027] (2) Pulverize the natural zeolite and heat-preserve it at 250°C for 50 minutes to obtain the pretreated zeolite;
[0028] (3) Add alkali solution to ethanol aqueous solution of tetraethyl orthosilicate, control the pH to 9, then add lithium nitrate, stir and react at 73°C for 2 hours, mix the obtained solution with pretreated zeolite at a mass ratio of 13:1, and store at room temperature 1. Stir and mix for 60 minutes under the condition of rotating speed 350r / min and filter to obtain modified zeolite;
[0029] (4) Mix graphite and oxidant at a mass ratio of 1:5, then stir and react, then concentrate by rotary evaporation to obtain graphite oxide;
Embodiment 2
[0033] A preparation method for building tile grout, comprising the following steps:
[0034] (1) Dissolve polyvinyl alcohol in an aqueous ethanol solution with a mass fraction of 30% at 87°C, and then add a water-soluble resin solution to obtain polyvinyl alcohol glue;
[0035] (2) Pulverize the natural zeolite and heat-preserve it at 230°C for 60 minutes to obtain the pretreated zeolite;
[0036] (3) Add alkali solution to ethanol aqueous solution of tetraethyl orthosilicate, control the pH to 10, then add lithium nitrate, stir and react at 70°C for 1 hour, mix the obtained solution with pretreated zeolite at a mass ratio of 10:1, and store at room temperature 1. Stir and mix for 70 minutes under the condition of rotating speed 400r / min and filter to obtain modified zeolite;
[0037] (4) Mix graphite and oxidant at a mass ratio of 1:4, stir and react, and concentrate by rotary evaporation to obtain graphite oxide;
[0038] (5) Take 35 parts of cement, 40 parts of quartz sa...
Embodiment 3
[0041] A preparation method for building tile grout, comprising the following steps:
[0042] (1) Dissolve polyvinyl alcohol in an aqueous ethanol solution with a mass fraction of 10% at 95°C, and then add a water-soluble resin solution to obtain polyvinyl alcohol glue;
[0043] (2) Pulverize the natural zeolite and heat-preserve it at 260°C for 40 minutes to obtain the pretreated zeolite;
[0044] (3) Add alkali solution to ethanol aqueous solution of tetraethyl orthosilicate, control the pH to 8, then add lithium nitrate, stir and react at 75°C for 3 hours, mix the obtained solution with pretreated zeolite at a mass ratio of 15:1, and store at room temperature 1. Stir and mix for 70 minutes under the condition of rotating speed 300r / min and filter to obtain modified zeolite;
[0045] (4) Mix graphite and oxidant at a mass ratio of 1:6, then stir and react, then concentrate by rotary evaporation to obtain graphite oxide;
[0046] (5) Take 50 parts of cement, 50 parts of quart...
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