Method for preparing artificial soil through mixed pyrolysis of lead-copper tailings and crop straw
A technology for crop straw and artificial soil is applied in the field of mixed pyrolysis of lead-copper tailings and crop straw to prepare artificial soil, which can solve the problems of limited adsorption sites for remediation agents, low heavy metal adsorption capacity, and inability to remove sulfur elements, etc. Achieving the effect of high heavy metal adsorption
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Embodiment 1
[0033] The method for preparing artificial soil by mixing and pyrolyzing lead-copper tailings and crop stalks comprises the following steps:
[0034] S1. Mix the crop straw powder and orthophosphate evenly, then add lead-copper tailings powder and mix evenly to obtain a mixture. The mass ratio of orthophosphate, crop straw powder and lead-copper tailings powder is 1:20:500;
[0035] S2. Pyrolyze the mixture obtained in step S1. Nitrogen gas is introduced at a flow rate of 200mL / min before pyrolysis to present an anaerobic state. The heating rate of pyrolysis is 10°C / min. When the temperature reaches 300°C, keep the temperature for 1h, and then Cool to room temperature;
[0036] S3. Take out the pyrolysis product, add bottom mud or sludge to the pyrolysis product and mix evenly to obtain artificial soil. The mass ratio of pyrolysis product to bottom mud or sludge is 80:1.
Embodiment 2
[0038] The method for preparing artificial soil by mixing and pyrolyzing lead-copper tailings and crop stalks comprises the following steps:
[0039] S1. Mix crop straw powder and orthophosphate evenly, then add lead-copper tailings powder and mix uniformly to obtain a mixture. The mass ratio of orthophosphate, crop straw powder and lead-copper tailings powder is 1:50:1000;
[0040] S2. Pyrolyze the mixture obtained in step S1. Nitrogen gas is introduced at a flow rate of 200mL / min before pyrolysis to present an anaerobic state. The pyrolysis heating rate is 20°C / min. When the temperature reaches 500°C, keep the temperature for 3h, and then Cool to room temperature;
[0041] S3. Take out the pyrolysis product, add bottom mud or sludge to the pyrolysis product and mix evenly to obtain artificial soil. The mass ratio of pyrolysis product to bottom mud or sludge is 120:1.
Embodiment 3
[0043] The method for preparing artificial soil by mixing and pyrolyzing lead-copper tailings and crop stalks comprises the following steps:
[0044] S1. Mix the crop straw powder and orthophosphate evenly, then add lead-copper tailings powder and mix evenly to obtain a mixture. The mass ratio of orthophosphate, crop straw powder and lead-copper tailings powder is 1:35:750;
[0045] S2. Pyrolyze the mixture obtained in step S1. Nitrogen gas is introduced at a flow rate of 200mL / min before pyrolysis to present an anaerobic state. The heating rate of pyrolysis is 15°C / min. When the temperature reaches 400°C, keep the temperature for 2h, and then Cool to room temperature;
[0046] S3. Take out the pyrolysis product, add bottom mud or sludge to the pyrolysis product and mix evenly to obtain artificial soil, the mass ratio of pyrolysis product to bottom mud or sludge is 100:1.
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