Method for preparing bionic adhesive material based on micro-nano additive
A bionic adhesive and micro-nano technology, applied in the field of bionic adhesive materials, can solve the problems of high cost and time consumption, and achieve the effects of reducing preparation costs, solving adhesion, and reducing difficulty
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Embodiment 1
[0035] Preparation of Polydimethylsiloxane-based Mushroom-like Biomimetic Adhesive Material
[0036] Dibutyl adipate (DBA) and tetrahydrofuran (THF) are selected as the plasticizer and organic solvent in this embodiment, and other types of plasticizers and organic solvents have similar functions and effects.
[0037] Step 1, PVC gel solution configuration:
[0038] Add PVC powder, plasticizer (DBA), organic solvent (THF) into the conical flask at a mass ratio of 1:1.75:15, place it on a magnetic stirrer and stir at 500r / min for 5 minutes, then add PVC to the conical flask, Place on a magnetic stirrer and stir at 1500r / min for 24 hours to obtain a PVC gel solution;
[0039] Step 2, a mold inversion:
[0040] Place the additively manufactured micro-nano mold in a glass petri dish, pour the mold with PVC solution, and place it in a vacuum box after the solution is naturally leveled, remove air bubbles by vacuuming, and allow the PVC gel solution to fully penetrate into the mold...
Embodiment 2
[0045] Preparation of carbon nanotube-doped polydimethylsiloxane-based biomimetic adhesive materials
[0046] Dibutyl adipate (DBA) and tetrahydrofuran (THF) are selected as the plasticizer and organic solvent in this embodiment, and other types of plasticizers and organic solvents have similar functions and effects.
[0047] Step 1, PVC gel solution configuration:
[0048] Add PVC powder, plasticizer (DBA), organic solvent (THF) into the conical flask at a mass ratio of 1:1.75:15, place it on a magnetic stirrer and stir at 500r / min for 5 minutes, then add PVC to the conical flask, Place on a magnetic stirrer and stir at 1500r / min for 24 hours to obtain a PVC gel solution;
[0049] Step 2, a mold inversion:
[0050] Place the additively manufactured micro-nano mold in a glass petri dish, pour the mold with PVC solution, and place it in a vacuum box after the solution is naturally leveled, remove air bubbles by vacuuming, and allow the PVC gel solution to fully penetrate into...
Embodiment 3
[0055] Preparation of epoxy resin-based biomimetic adhesive materials:
[0056] Step 1, PVC gel solution configuration:
[0057] Add PVC powder, plasticizer (DBA), organic solvent (THF) into the conical flask at a mass ratio of 1:1.75:15, place it on a magnetic stirrer and stir at 500r / min for 5 minutes, then add PVC to the conical flask, Place on a magnetic stirrer and stir at 1500r / min for 24 hours to obtain a PVC gel solution;
[0058] Step 2, a mold inversion:
[0059] Select dibutyl adipate (DBA), tetrahydrofuran (THF) as the plasticizer and organic solvent of this example, and other types of plasticizers and organic solvents have similar functions and effects.
[0060] Place the additively manufactured micro-nano mold in a glass petri dish, pour the mold with PVC solution, and place it in a vacuum box after the solution is naturally leveled, remove air bubbles by vacuuming, and allow the PVC gel solution to fully penetrate into the mold ; Put the beaker into a glass a...
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