Heterocyclic organic electroluminescent material and preparation method, application and device thereof
A luminescent and electromechanical technology, applied in luminescent materials, electrical solid devices, organic chemistry, etc., can solve the problems of current efficiency, light color and life comprehensive performance not meeting industry standards, and achieve excellent light color and life, and luminous efficiency High, good thermal stability
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[0074] Embodiments of the present invention are described in detail below. The embodiments described below are exemplary only for explaining the present invention and should not be construed as limiting the present invention. If no specific technique or condition is indicated in the examples, it shall be carried out according to the technique or condition described in the literature in this field or according to the product specification. All reagents and instruments used are commercially available conventional products.
[0075] Synthesis Example 1: Synthesis of Compound (1)
[0076]
[0077] Step 1: Add 5.52 g (40 mmol) of potassium carbonate and 100 mL of xylene into a reaction flask containing 4.74 g (20 mmol) of 2,4-dichlorodibenzofuran and 8.36 g (50 mmol) of carbazole. Introduce nitrogen, add cuprous iodide 0.38g (2mmol) and o-phenanthroline 0.72g (4mmol), heat and reflux and stir for 8h. The temperature was cooled to room temperature, filtered, the liquid phase w...
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