Oral care composition containing probiotics and application of oral care composition containing probiotics
An oral care and composition technology, applied in the field of daily chemicals, can solve problems such as weak antibacterial activity, yellowing of toothpaste paste, and increase product instability, so as to improve inhibition ability, good curative effect, and avoid paste quality decline Effect
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Embodiment 1
[0030] Embodiment 1, the preparation of microcapsule
[0031] S1. Dissolving shellac resin in an aqueous sodium carbonate solution with a concentration of 0.1mol / L at 65°C to prepare a saturated shellac resin sodium salt solution, freeze-drying, and grinding to obtain shellac resin sodium salt for later use;
[0032] S2, dissolving carboxymethyl chitosan in water to prepare an aqueous carboxymethyl chitosan solution with a concentration of 0.5 mg / mL; dissolving shellac resin sodium salt in water to prepare a concentration of 3 mg / mL sodium shellac resin Saline solution; the above-mentioned carboxymethyl chitosan aqueous solution and shellac resin sodium salt aqueous solution were mixed, and at room temperature, magnetically stirred for 12 minutes to obtain a shellac resin sodium salt-chitosan complex; the carboxymethyl chitosan and The mass ratio of lac resin sodium salt is 0.22:1;
[0033] S3. Weigh the shellac resin sodium salt-chitosan complex, dissolve it in water, add p...
Embodiment 2
[0035] Embodiment 2, the preparation of microcapsule
[0036] S1. Dissolving shellac resin in an aqueous sodium carbonate solution with a concentration of 0.2 mol / L at 60°C to prepare a saturated shellac resin sodium salt solution, freeze-drying, and grinding to obtain shellac resin sodium salt, which is set aside;
[0037] S2, dissolving carboxymethyl chitosan in water to prepare an aqueous carboxymethyl chitosan solution with a concentration of 0.1 mg / mL; dissolving shellac resin sodium salt in water to prepare a concentration of 1 mg / mL sodium shellac resin Saline solution; the above-mentioned carboxymethyl chitosan aqueous solution and shellac resin sodium salt aqueous solution were mixed, and at room temperature, magnetically stirred for 10 minutes to obtain a shellac resin sodium salt-chitosan complex; the carboxymethyl chitosan and The mass ratio of lac resin sodium salt is 0.1:1;
[0038] S3. Weigh the lac resin sodium salt-chitosan complex, dissolve it in water, ad...
Embodiment 3
[0040] Embodiment 3, the preparation of microcapsule
[0041] S1. Dissolving shellac resin in an aqueous sodium carbonate solution with a concentration of 0.3 mol / L at 60° C. to prepare a saturated shellac resin sodium salt solution, freeze-drying, and grinding to obtain shellac resin sodium salt for later use;
[0042] S2, dissolving carboxymethyl chitosan in water to prepare an aqueous carboxymethyl chitosan solution with a concentration of 1 mg / mL; dissolving shellac resin sodium salt in water to prepare a concentration of 3 mg / mL shellac resin sodium salt aqueous solution; the above-mentioned carboxymethyl chitosan aqueous solution and lac resin sodium salt aqueous solution were mixed, and at room temperature, magnetically stirred for 10 minutes to obtain a shellac resin sodium salt-chitosan complex; the carboxymethyl chitosan and violet The mass ratio of gum resin sodium salt is 0.35:1;
[0043] S3. Weigh the lac resin sodium salt-chitosan complex, dissolve it in water, ...
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