Preparation method of carbon nanotube reinforced aluminum alloy semi-solid slurry
A semi-solid slurry and carbon nanotube technology, which is applied in the field of metal material manufacturing, can solve the problems of metal melt contamination and corrosion, magnetic flux leakage, expensive stirring equipment, etc., and achieves uniform secondary phase distribution, safe operation, and good bonding. Effect
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Embodiment 1
[0030] A method for preparing carbon nanotube reinforced aluminum alloy semi-solid slurry, comprising the following steps:
[0031] (1) Mix an appropriate amount of carbon nanotubes with an outer diameter of 20-60nm, a length of 10-30μm, and a purity of ≥99.5% with absolute ethanol in a beaker, mixing 3.0g of carbon nanotubes per 100ml of ethanol, and then put them into an ultrasonic Perform ultrasonic dispersion treatment in the instrument for 120min, the ultrasonic power is 450W, and the frequency is 40kHz; the purity is ≥99.9%, the particle size is 100-200 mesh aluminum powder, potassium tetrafluoroaluminate powder and absolute ethanol are mixed in a beaker at a rate of 150ml of ethanol 45g of aluminum powder and 3.0g of potassium tetrafluoroaluminate were mixed by mechanical stirring for 120min at a stirring speed of 120r / min; then, the mixed and dispersed aluminum powder-tetrafluoroaluminate was evenly added to the carbon nanotube ethanol dispersion after ultrasonic Conti...
Embodiment 2
[0039] A method for preparing carbon nanotube reinforced aluminum alloy semi-solid slurry, comprising the following steps:
[0040] (1) Mix an appropriate amount of carbon nanotubes with an outer diameter of 20-60nm, a length of 10-30μm, and a purity of ≥99.5% with absolute ethanol in a beaker, mixing 2.5g of carbon nanotubes per 100ml of ethanol, and then put them into an ultrasonic Perform ultrasonic dispersion treatment in the instrument for 100min, the ultrasonic power is 400W, and the frequency is 35kHz; the purity ≥ 99.9%, the particle size is 100-200 mesh aluminum powder, potassium tetrafluoroaluminate powder and absolute ethanol in a beaker at a rate of 150ml of ethanol solution Mix 40g of aluminum powder and 2.5g of potassium tetrafluoroaluminate for 100min by mechanical stirring at a stirring speed of 100r / min; then add the mixed and dispersed aluminum powder-tetrafluoroaluminum evenly into the carbon nanotube ethanol dispersion after ultrasonic Continue to ultrasoni...
Embodiment 3
[0048] A method for preparing carbon nanotube reinforced aluminum alloy semi-solid slurry, comprising the following steps:
[0049] (1) Mix an appropriate amount of carbon nanotubes with an outer diameter of 20-60nm, a length of 10-30μm, and a purity of ≥99.5% with absolute ethanol in a beaker with 3.5g of carbon nanotubes per 100ml of ethanol, and then put them into an ultrasonic Perform ultrasonic dispersion treatment in the instrument for 150min, the ultrasonic power is 480W, and the frequency is 45kHz; the purity ≥ 99.9%, the particle size is 100-200 mesh aluminum powder, potassium tetrafluoroaluminate powder and absolute ethanol are mixed in a beaker at a rate of 150ml of ethanol 50g of aluminum powder and 3.5g of potassium tetrafluoroaluminate were mixed by mechanical stirring for 150min at a stirring speed of 140r / min; then, the mixed and dispersed aluminum powder-tetrafluoroaluminate was evenly added to the carbon nanotube ethanol dispersion after ultrasonic Continue t...
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