Photo-thermal material based on porous carbon spheres and preparation method thereof
A porous carbon, photothermal technology, applied in the preparation/purification of carbon, chemical instruments and methods, general water supply saving, etc., can solve the problems of limiting the practical application of the technology, poor hydrophilicity of photothermal materials, low photothermal conversion efficiency, etc. , to achieve the effect of mild conditions, simple preparation method and convenient operation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] 0.54g Na 2 MoO 4 Disperse 5.89g of glucose in 57.5ml deionized water, ultrasonically disperse, and magnetically stir at room temperature to obtain a uniform solution A; drop 2.5ml of concentrated hydrochloric acid into solution A, and magnetically stir at room temperature to obtain a uniform solution B; then transfer the mixed solution B to In a hydrothermal reaction kettle, react at a constant temperature of 180°C for 6h, wash, and freeze-dry at -50°C for 35h to obtain a carbon sphere photothermal material precursor.
[0038] The obtained carbon sphere photothermal material precursor was placed in a tube furnace, annealed at 800°C for 2 hours in an argon atmosphere, and the heating rate was 5°C / min; then it was annealed at 300°C for 2 hours in an air atmosphere, and the heating rate was 1°C / min; get MoO 3 porous carbon spheres; subsequently, the obtained MoO 3 The porous carbon spheres were dispersed in ammonia solution, magnetically stirred for 12 hours, and the Mo...
Embodiment 2
[0041] 0.72g Na 2 MoO 4 Disperse 5.89g of glucose in 57.5ml deionized water, ultrasonically disperse, and magnetically stir at room temperature to obtain a uniform solution A; drop 2.5ml of concentrated hydrochloric acid into solution A, and magnetically stir at room temperature to obtain a uniform solution B; then transfer the mixed solution B to In a hydrothermal reaction kettle, react at a constant temperature of 180°C for 6h, wash, and freeze-dry at -50°C for 35h to obtain a carbon sphere photothermal material precursor.
[0042] The obtained carbon sphere photothermal material precursor was placed in a tube furnace, annealed at 800°C for 2 hours in an argon atmosphere, and the heating rate was 5°C / min; then it was annealed at 300°C for 2 hours in an air atmosphere, and the heating rate was 1°C / min; get MoO 3 porous carbon spheres; subsequently, the obtained MoO 3 The porous carbon spheres were dispersed in ammonia solution, magnetically stirred for 12 hours, and the Mo...
Embodiment 3
[0045] 0.54g Na 2 MoO 4 Disperse 5.89g of glucose in 57.5ml deionized water, ultrasonically disperse, and magnetically stir at room temperature to obtain a uniform solution A; drop 2.5ml of concentrated hydrochloric acid into solution A, and magnetically stir at room temperature to obtain a uniform solution B; then transfer the mixed solution B to In a hydrothermal reaction kettle, react at a constant temperature of 180°C for 6h, wash, and freeze-dry at -50°C for 35h to obtain a carbon sphere photothermal material precursor.
[0046] The obtained carbon sphere photothermal material precursor was put into a tube furnace, annealed at 800°C for 2 hours in an ammonia atmosphere, and the heating rate was 5°C / min; then annealed at 300°C for 2 hours in an air atmosphere, and the heating rate was 1°C / min; get MoO 3 N-doped porous carbon spheres; subsequently, the obtained MoO 3 The N-doped porous carbon spheres were dispersed in ammonia solution, stirred magnetically for 12 hours, ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| diameter | aaaaa | aaaaa |
| diameter | aaaaa | aaaaa |
| diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More