Aqueous battery
A water-based electrolyte and battery technology, applied in secondary batteries, water-based electrolytes, circuits, etc., can solve the problems of reducing ion diffusion rate and high cost, and achieve the effect of improving electrochemical window, low cost, and improving energy density
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Embodiment 1
[0050] Preparation of Na by co-precipitation 1.87 mn 0.78 [Fe(CN) 6 ]·2.1H 2 O is used as the positive electrode active material and prepares the positive electrode sheet. The specific preparation process is as follows: 50 milliliters of 0.2mol / L sodium ferrocyanide solution (if no special instructions, all use water as solvent) and 50 milliliters of 0.2mol / L sodium ferrocyanide solution The manganese sulfate solution is injected into 100 milliliters of 0.3mol / L disodium ethylenediaminetetraacetic acid solution at the same time, and at 60°C, the positive active material is obtained through co-precipitation reaction; the positive active material, conductive carbon, and polyvinylidene fluoride are The ratio of 7:2:1 is mixed evenly, and the positive electrode sheet is obtained by stirring, coating, drying, and rolling.
[0051] Assemble the positive pole piece, zinc sheet, and water-based electrolyte into a water-based battery. The solvent in the water-based electrolyte used ...
Embodiment 2
[0058] The preparation of the positive electrode sheet is the same as in Example 1. The positive electrode sheet, zinc sheet, and aqueous electrolyte are assembled into an aqueous battery. The solvent in the aqueous electrolyte used is heavy water, and the solute is 1mol / kg NaCF 3 SO 3 , 0.1mol / kg of Zn(CF 3 SO 3 ) 2 , and 6mol / kg of Na 2 C 4 h 8 o 8 . The battery was cycled for 100 times at a voltage range of 0.2-2.15V and a current of 5C, and the capacity retention rate was 71%.
Embodiment 3
[0060] Preparation of K by ion exchange method 1.77 Fe[Fe(CN) 6 ] 0.94 1.2H 2 O is used as the positive electrode active material and prepares the positive electrode sheet. The specific preparation process is as follows: 50 milliliters of 0.2mol / L potassium ferrocyanide solution (if no special instructions, all use water as solvent) and 50 milliliters of 0.2mol / L potassium ferrocyanide solution Ferrous sulfate solution injects in the disodium edetate solution of 0.3mol / L of 100 milliliters simultaneously, at room temperature obtains positive active material through coprecipitation reaction; Positive active material, conductive carbon, polyvinylidene fluoride are weighed The ratio of 7:2:1 is mixed evenly, and the positive electrode sheet is obtained by stirring, coating, drying, and rolling.
[0061] Assemble the positive electrode sheet, zinc sheet, and water-based electrolyte into a water-based battery. The water-based electrolyte used is heavy water as a solvent, and the...
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