Preparation method of ultrahigh-Bs low-loss manganese zinc ferrite material for cloud computing
A manganese-zinc ferrite and low-loss technology, which is applied in the field of preparation of ultra-high Bs and low-loss manganese-zinc ferrite materials for cloud computing, can solve unfavorable saturation magnetic induction intensity, low sintered density of products, and decreased material resistivity, etc. Problems, achieve the effect of reducing volume and loss, reducing loss, and reducing sintering temperature
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[0038] In the first aspect, the embodiment of the present application also provides a method for preparing an ultra-high Bs low-loss manganese-zinc ferrite material for cloud computing, such as figure 1 shown, including the following steps:
[0039] Step S10, Fe 2 o 3 , ZnO, Mn 3 o 4 Mixing to obtain a precursor material, the precursor material includes 62.0mol% to 66.0mol% of Fe 2 o 3 , 17.0mol%~19.0mol% of ZnO and the balance of Mn 3 o 4 and performing wet ball milling after mixing the precursor material, water and binder to obtain the first slurry;
[0040] Step S20, performing spray granulation on the first slurry to obtain a first granular material;
[0041] Step S30, pre-sintering the first granular material to obtain a second granular material;
[0042] Step S40, mixing the second granular material, water, binder and additives and performing wet ball milling to obtain a second slurry, wherein the additives include a mass percentage of the second granular materi...
Embodiment 1
[0097] Ingredients: Fe 2 o 3 The content of ZnO is 62.5mol%, the content of ZnO is 18.5mol%, and the rest is Mn 3 o 4 Proceed with the batching of the main ingredients. The doped oxide includes 150-400ppm of CaO and 80-250ppm of SiO in terms of mass fraction 2 , 200~600ppm V 2 o 5 , 200~450ppm of SnO 2 , 100~350ppm TiO 2 Dosing of additives.
[0098] Feeding and mixing: In the process of feeding, half of the Fe is fed first 2 o 3 , after feeding ZnO and Mn 3 o 4 , and cast the other half Fe 2 o 3 , mixing the materials evenly, wet grinding and sand grinding to obtain the first slurry; spraying and granulating the first slurry to obtain the spherical first granular material.
[0099] The first granular material is sintered in a segmented atmosphere, the pre-fired temperature is controlled at 900-980°C, kept for 2 hours, and the sintering method is oxidized at 800-600°C in the cooling section, and the oxygen content is controlled at 21-21. 25%, the material fully ...
Embodiment 2
[0104] According to the preparation method of embodiment 1, sample S2 is obtained, and the difference from embodiment 1 is that during batching, Fe 2 o 3 The content of ZnO is 65mol%, the content of ZnO is 17.5mol%, and the rest is Mn 3 o 4 and doped oxides.
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