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Walnut peptide-chitosan-sodium alginate composite membrane as well as preparation method and application thereof

A sodium alginate film and sodium alginate technology are applied in the field of edible films, which can solve the problems affecting the performance of composite films and adverse reactions of components, and achieve the effect of improving barrier properties and mechanical properties.

Active Publication Date: 2021-08-20
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The common composite methods in current research include direct blending of materials and layer-by-layer assembly of each material. Direct blending is simple and convenient, but adverse reactions may occur between components, which will affect the performance of composite membranes.

Method used

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  • Walnut peptide-chitosan-sodium alginate composite membrane as well as preparation method and application thereof
  • Walnut peptide-chitosan-sodium alginate composite membrane as well as preparation method and application thereof
  • Walnut peptide-chitosan-sodium alginate composite membrane as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0054] 1. Preparation of Sodium Alginate Monolayer Membrane

[0055] Weigh 1.50g of sodium alginate, slowly add sodium alginate into 100mL of distilled water while stirring, magnetically stir in a water bath at 40°C for 1h until it is completely dissolved, then add 2mL of glycerin, stir evenly to make a 100mL membrane solution, put into ultrasonic Degassed in a washer for 10 minutes, set aside. Pour 15g of sodium alginate solution into a plastic petri dish with a diameter of 90mm, spread it evenly, and then place it in a constant temperature blast drying oven at 30°C for 24 hours to form a film.

[0056] 2. Preparation of Chitosan-Walnut Peptide Covalent Complex

[0057] Weigh 1.5 g of chitosan powder and dissolve it in 1% (v / v, %) acetic acid solution, and magnetically stir until completely dissolved. Weigh 0.5g of walnut peptide powder and dissolve in distilled water, and stir magnetically in a water bath at 60°C for 30min. The walnut peptide aqueous solution was mixed wi...

Embodiment 2

[0061] 1. Preparation of Sodium Alginate Monolayer Membrane

[0062] Weigh 1.50g of sodium alginate, slowly add sodium alginate into 100mL of distilled water while stirring, magnetically stir in a water bath at 40°C for 1h until it is completely dissolved, then add 2mL of glycerin, stir evenly to make a 100mL membrane solution, put into ultrasonic Degassed in a washer for 10 minutes, set aside. Pour 15g of sodium alginate solution into a plastic petri dish with a diameter of 90mm, spread it evenly, and then place it in a constant temperature blast drying oven at 30°C for 24 hours to form a film.

[0063] 2. Preparation of Chitosan-Walnut Peptide Covalent Complex

[0064] Weigh 1 g of chitosan powder and dissolve it in 1% (v / v, %) acetic acid solution, and magnetically stir until completely dissolved. Weigh 1g of walnut peptide powder and dissolve it in distilled water, and magnetically stir in a water bath at 60°C for 30min. The walnut peptide aqueous solution was mixed wit...

Embodiment 3

[0068] 1. Preparation of Sodium Alginate Monolayer Membrane

[0069] Weigh 1.50g of sodium alginate, slowly add sodium alginate into 100mL of distilled water while stirring, magnetically stir in a water bath at 40°C for 1h until it is completely dissolved, then add 2mL of glycerin, stir evenly to make a 100mL membrane solution, put into ultrasonic Degassed in a washer for 10 minutes, set aside. Pour 15g of sodium alginate solution into a plastic petri dish with a diameter of 90mm, spread it evenly, and then place it in a constant temperature blast drying oven at 30°C for 24 hours to form a film.

[0070] 2. Preparation of Chitosan-Walnut Peptide Covalent Complex

[0071] Weigh 0.5 g of chitosan powder and dissolve it in 1% (v / v, %) acetic acid solution, and magnetically stir until completely dissolved. Weigh 1.5g of walnut peptide powder and dissolve in distilled water, and stir magnetically in a water bath at 60°C for 30min. The walnut peptide aqueous solution was mixed wi...

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Abstract

The invention relates to a walnut peptide-chitosan-sodium alginate composite membrane as well as a preparation method and application thereof. The composite membrane comprises a sodium alginate membrane and a chitosan-walnut peptide membrane, the sodium alginate membrane comprises sodium alginate, and the chitosan-walnut peptide membrane comprises a covalent cross-linked compound formed by chitosan and walnut peptide. The problem that a food packaging material is not easy to degrade is solved, the food preservation problem is solved, the problems that an edible film is poor in moisture resistance and mechanical performance are solved, and the problem that a composite membrane is reduced in performance is solved.

Description

technical field [0001] The invention belongs to the technical field of edible films, and in particular relates to a walnut peptide-chitosan-sodium alginate composite film and a preparation method and application thereof. Background technique [0002] The information disclosed in this background section is only intended to increase the understanding of the general background of the present invention, and is not necessarily taken as an acknowledgment or any form of suggestion that the information constitutes the prior art already known to those skilled in the art. [0003] Edible film refers to the biodegradable and edible film formed by the interaction between molecules, which is made of natural edible macromolecular substances and added with edible plasticizers, crosslinking agents and other substances. As a carrier for certain functional ingredients. Edible film can be covered on the surface of food by wrapping, dipping or spraying to reduce the contact between food and mo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J7/048C08J5/18C08L5/04C08K5/053C08L5/08C08L89/00C08K5/1545B65D65/46
CPCC08J7/048C08J7/0427C08J5/18B65D65/463B65D65/466C08J2305/04C08K5/053C08J2305/08C08J2405/08C08J2389/00C08J2489/00C08K5/1545
Inventor 陈浩刘文昕
Owner SHANDONG UNIV