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The heating and cooling cycle heat treatment method near the initial melting temperature of the primary precipitation phase of the cast alloy

A heat treatment method and casting magnesium alloy technology, which is applied in the field of heating and cooling cycle heat treatment near the initial melting temperature of the primary precipitation phase of cast alloys, to achieve the effects of wide application range, optimized structure, and improved alloy performance

Active Publication Date: 2022-08-09
SHANGHAI JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of the lack of a universal and efficient method for improving the coarse and sharp morphology of the primary precipitates in cast alloys in the prior art, the purpose of the present invention is to provide a simple, efficient and universal primary precipitates of cast alloys Cyclic heat treatment method, that is, the alloy to be heat treated is subjected to heating and cooling cycle heat treatment near the initial melting temperature of the primary precipitation phase, and the microstructure and comprehensive mechanical properties of the cast alloy are improved to the greatest extent by the most economical means

Method used

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  • The heating and cooling cycle heat treatment method near the initial melting temperature of the primary precipitation phase of the cast alloy
  • The heating and cooling cycle heat treatment method near the initial melting temperature of the primary precipitation phase of the cast alloy
  • The heating and cooling cycle heat treatment method near the initial melting temperature of the primary precipitation phase of the cast alloy

Examples

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Embodiment 1

[0031] Example 1: Metal mold gravity casting aluminum-zinc-magnesium-copper-chromium alloy cyclic heat treatment at 481°C for 5 times

[0032] The material used in this embodiment is aluminum-zinc-magnesium-copper-chromium cast aluminum alloy, and its chemical composition is: 5% magnesium, 3% zinc, 1% copper, 2% chromium, 78.6% aluminum, 0.2% iron, and 0.2% silicon. %; the initial melting temperature of the primary precipitation phase of the aluminum-zinc-magnesium-copper-chromium cast aluminum alloy is 481 ℃: using a crucible resistance furnace to melt Al-5wt.%Mg-3wt.%Zn-1wt.%Cu-2wt. %Cr-0.2wt.%Fe-0.2wt.%Si alloy, pour the alloy liquid into a metal mold to obtain an ingot with a size of 150mm×100mm×20mm, and then cut out 10mm×10mm×10mm in the center of the ingot The sample is processed as follows:

[0033] The samples were heated from room temperature to 491°C at a ramp rate of 10°C / min in a programmable air circulation oven, followed by holding at 491°C for 5 min. Then, th...

Embodiment 2

[0034] Example 2: Metal mold low-pressure casting aluminum-silicon alloy heat treatment for 20 cycles of heating and cooling at around 577°C

[0035]The materials used in this embodiment are aluminum-silicon cast aluminum alloys, and the aluminum-silicon cast aluminum alloys contain components and mass ratios as follows: silicon 20%, and the rest is aluminum (80%); the cast Al-20wt.%Si alloy The initial melting temperature of the primary precipitation phase is 577 °C: the Al-20wt.%Si alloy is smelted in a graphite crucible using a crucible resistance furnace, and then a disc-shaped part with a size of Φ350mm × 120mm is obtained by metal mold low-pressure casting. A sample of 10mm × 10mm × 10mm is cut from the center of the casting, and the sample is processed as follows:

[0036] The sample was heated from room temperature to 587°C at a heating rate of 5°C / min, followed by incubation at 587°C for 30 min. Then, the sample was cooled to 567°C at a cooling rate of 5°C / min, and k...

Embodiment 3

[0037] Example 3: Centrifugal casting of aluminum-magnesium-erbium alloy heating and cooling cycles around 450°C for 10 times

[0038] The materials used in this embodiment are aluminum-magnesium-erbium cast aluminum alloys, and the aluminum-magnesium-erbium cast aluminum alloys contain components and mass ratios as follows: magnesium 5%, erbium 0.5%, and the rest is aluminum (94.5%); the cast Al-5wt %Mg-0.5wt.%Er alloy's primary precipitation initial melting temperature is 450℃: Al-5wt.%Mg-0.5wt.%Er alloy was smelted in a graphite crucible using a crucible resistance furnace, followed by centrifugation in a metal-type bedroom Casting method The casting is formed to obtain a casting with a size of Φ300mm × 400mm, and then a sample of 10mm × 10mm × 10mm is cut out of the casting, and the sample is processed as follows:

[0039] The sample was heated from room temperature to 455°C at a ramp rate of 5°C / min, followed by incubation at 455°C for 30 min. Then, the sample was cooled...

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Abstract

The invention provides a heating and cooling cyclic heat treatment method near the initial melting temperature of the primary precipitation phase of a casting alloy, and the casting alloy is subjected to cyclic heating and cooling treatment near the initial melting temperature of the primary precipitation phase. Taking advantage of the fact that the interfacial energy between the primary precipitation phase and the alloy matrix is ​​high, and the sharper the primary precipitation phase is, the higher the interface energy is, and the more likely the initial melting occurs. Initial melting occurs, and then the temperature is lowered to solidify and passivate the primary precipitation after the initial melting, and the primary precipitation is repeatedly subjected to the initial melting-solidification passivation process by cyclic heating and cooling treatment; , flakes, sharp long needles and other shapes become passivated, round and small, which solves the shortcomings of ordinary heat treatment, such as the heating temperature is lower than the solidus temperature, and it is difficult to improve the low plasticity of the alloy caused by the coarse and sharp primary precipitates. , while optimizing the microstructure and improving the alloy properties.

Description

technical field [0001] The invention belongs to the technical field of heat treatment of metal materials, and in particular relates to a heating and cooling cycle heat treatment method near the initial melting temperature of a primary precipitation phase of a casting alloy. Background technique [0002] Cast aluminum alloy and magnesium alloy are widely used in automobile, aerospace and other industries due to their advantages of low density and high specific strength. A variety of primary precipitation phases are often inevitably formed in cast alloys, and these primary precipitation phases often exhibit elongated, slender needle-like, dendritic and other morphologies, and are often sharp in shape and coarse in size. These primary precipitates will seriously split the matrix structure and have a great adverse effect on the comprehensive mechanical properties of the alloy, which has attracted great attention of scientific and technological workers. [0003] At present, in o...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/04C22F1/06C22C21/08C22F1/047C22C21/02C22F1/043C22C23/02
CPCC22F1/04C22F1/06C22C21/08C22F1/047C22C21/02C22F1/043C22C23/02Y02P10/25
Inventor 王渠东雷川魏杰
Owner SHANGHAI JIAOTONG UNIV