Anthryl organic porous polymer and synthesis method thereof and application of anthryl organic porous polymer in kanamycin detection
A technology of a porous polymer and a synthesis method is applied in the application field of anthracene-based organic porous polymer and its synthesis, detection of kanamycin, and achieves the effects of good stability, good reproducibility and high yield
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Embodiment 1
[0047] The synthesis method of the above-mentioned anthracene organic porous polymer includes the following steps:
[0048]The α, α'- dibromo-p-xylene and placed in a round bottom flask anthracene, round bottom flask was added methylene chloride and stirred at room temperature for 20 ~ 25 ℃ 5 minutes to obtain the supernatant. And then purged with nitrogen, was added anhydrous aluminum chloride under nitrogen atmosphere, which was placed in an oil bath for 2 days at 40 ℃ stirred (24 hours, the temperature remains constant per day), naturally down to room temperature 20 to 25 ℃, the solid was filtered to give a brown powder as the organic porous polymer anthryl, washed with water anthryl organic porous polymer, producing dried for one day (at room temperature 20 ~ 25 ℃), anthryl organic porous polymer was washed in the air 98%, wherein the amount of substance anthracenes 1.0mmol, α, α'- dibromo-p-xylene as the amount of substance 1.1 mmol, the amount of substance of anhydrous alumi...
Embodiment 2
[0051] The method of synthesizing the above organic porous polymer anthryl, comprising the steps of:
[0052] The α, α'- dibromo-p-xylene and placed in a round bottom flask anthracene, round bottom flask was added methylene chloride and stirred at room temperature for 20 ~ 25 ℃ 5 minutes to obtain the supernatant. And then purged with nitrogen, was added anhydrous aluminum chloride under nitrogen atmosphere, which was placed in an oil bath for 3 days reaction at 40 ℃ stirred (24 hours, the temperature remains constant per day), naturally down to room temperature 20 to 25 ℃, the solid was filtered to give a brown powder as the organic porous polymer anthryl, washed with water anthryl organic porous polymer, producing dried for one day (at room temperature 20 ~ 25 ℃), anthryl organic porous polymer was washed in the air 96%, wherein the amount of substance anthracenes 1.1mmol, α, α'- dibromo-p-xylene as the amount of substance 1.2 mmol, anhydrous aluminum chloride in an amount of su...
Embodiment 3
[0055] The method of synthesizing the above organic porous polymer anthryl, comprising the steps of:
[0056] The α, α'- dibromo-p-xylene and placed in a round bottom flask anthracene, round bottom flask was added methylene chloride and stirred at room temperature for 20 ~ 25 ℃ 5 minutes to obtain the supernatant. And then purged with nitrogen, was added anhydrous aluminum chloride under nitrogen atmosphere, which was placed in an oil bath for 4 days reaction at 40 ℃ stirred (24 hours, the temperature remains constant per day), naturally down to room temperature 20 to 25 ℃, the solid was filtered to give a brown powder as the organic porous polymer anthryl, washed with water anthryl organic porous polymer, producing dried for one day (at room temperature 20 ~ 25 ℃), anthryl organic porous polymer was washed in the air 99%, wherein the amount of substance anthracenes 1.3mmol, α, α'- dibromo-p-xylene as the amount of substance 1.6 mmol, the amount of substance of anhydrous aluminum ...
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