Surface treatment liquid for coated steel plate, preparation method and use method
A technology of surface treatment liquid and coated steel plate, which is applied in the direction of surface coating liquid device, pretreatment surface, coating, etc., can solve the problems of poor bonding performance of zinc-aluminum-magnesium coated steel plate, etc.
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[0054] According to another typical embodiment of the present invention, a method for preparing any one of the above-mentioned surface treatment liquids for coated steel sheets is provided, comprising the following steps:
[0055] S0, preparing active side group polysiloxane.
[0056] Specifically, the preparation method of the active side group polysiloxane comprises the following steps:
[0057] Mix and heat polymethylhydrogensiloxane, alcohols, allyl compounds containing amine or epoxy groups and catalysts in an inert atmosphere (such as nitrogen atmosphere) to obtain the active side-group polysiloxane.
[0058] Wherein: the polymethylhydrogensiloxane is linear, the number average relative molecular mass of the polymethylhydrogensiloxane is 600-6000; the side group of the polymethylhydrogensiloxane contains silicon hydrogen Functional group and silicon methyl group, the mass molar concentration of described silicon hydrogen functional group is 1.5-1.6mol / 100g;
[0059] Th...
Embodiment 1
[0085] The present embodiment provides a kind of surface treatment liquid that is used for coated steel plate, and its preparation method comprises the following steps:
[0086] S0, preparing active side group polysiloxane.
[0087]10g polymethylhydrogen siloxane, 4.6g dehydrated alcohol, 4g allyl glycidyl ether with a mass molar concentration of 1.55mol / 100g of silicon hydrogen functional group were fully mixed (i.e. silicon hydrogen functional group, ethanol, allyl shrink The molar ratio of glycerol ether is 1:0.65:0.22), add 0.01g of Castel catalyst in an inert atmosphere, fully stir at 50°C for 6h, and filter to obtain a clear liquid that is the active side group polysiloxane.
[0088] S1. Mix the active side-group polysiloxane with the water-alcohol mixed solution to obtain a preformed solution.
[0089] Take 0.4 parts of the active side-group polysiloxane prepared in step S0, and add it dropwise to 100 parts of water-alcohol mixture (the mass ratio of water and ethanol ...
Embodiment 2
[0095] The present embodiment provides a kind of surface treatment liquid that is used for coated steel plate, and its preparation method comprises the following steps:
[0096] S0, preparing active side group polysiloxane.
[0097] The mass molar concentration of 10g silicon hydrogen functional group is 1.55mol / 100g polymethylhydrogen siloxane, 3.6g methanol, 2g allylamine are fully mixed (the molar ratio of silicon hydrogen functional group, methyl alcohol, allylamine is 1:0.73: 0.23), add 0.1 g of chloroplatinic acid in an inert atmosphere, and fully stir at room temperature for 8 h to obtain active side-group polysiloxane.
[0098] S1. Mix the active side-group polysiloxane with the water-alcohol mixed solution to obtain a preformed solution.
[0099] Take 0.07 parts of the active side-group polysiloxane prepared in step S0, and add it dropwise to 100 parts of water-alcohol mixture (the mass ratio of water and methanol is 1:1) at a rate of 10-100 drops / min. A stirring sp...
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