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Preparation method of water dispersible granules containing pyraclostrobin and dimethomorph

A technology of pyraclostrobin and dimethomorph, which is applied in the field of pesticides, can solve the problems of reducing the content of pyraclostrobin and dimethomorph, the influence of the bactericidal effect of fungicides, and the inability to solve the problems, so as to shorten the disintegration time, shorten the wetting time, and improve the effect of the control effect

Active Publication Date: 2022-07-12
山东百农思达生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, in the process of compounding pyraclostrobin and dimethomorph with plant growth regulators into water-dispersible granules, the following problems are prone to occur: the heat resistance of plant growth regulators is poor, and the high temperature of water-dispersible granules The activity of plant growth regulators will be affected during granulation and drying; the addition of plant growth regulators will affect the suspension stability of water-dispersible granules, which need to be prepared and used immediately; the addition of plant growth regulators will affect water dispersion The disintegration and suspension rate of granules requires adding more disintegrants and dispersants, which reduces the content of pyraclostrobin and dimethomorph, resulting in the inability to produce pyraclostrobin and dimethomorph Water-dispersible granules with low morphine content; pyraclostrobin and dimethomorph are prone to phytotoxicity during use, although plant growth regulators can reduce phytotoxicity, but the plant growth regulator after compounding to form water-dispersible granules The effect is slow and cannot alleviate the initial drug damage
[0007] In order to solve the above problems, the most commonly used method is to modify the dispersant and disintegrant and add synergist to enhance the effect of plant growth regulator, but it still cannot solve the problem of high temperature granulation and drying process on plant growth regulation. The activity of the fungicide is affected, and it cannot solve the problem of not being able to produce water-dispersible granules with high content of pyraclostrobin and dimethomorph, and the addition of synergists will also affect the bactericidal effect of the fungicide

Method used

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  • Preparation method of water dispersible granules containing pyraclostrobin and dimethomorph
  • Preparation method of water dispersible granules containing pyraclostrobin and dimethomorph
  • Preparation method of water dispersible granules containing pyraclostrobin and dimethomorph

Examples

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Embodiment 1

[0039] A preparation method of a water-dispersible granule containing pyraclostrobin and dimethomorph, specifically:

[0040] 1. Preparation of a mixture: add pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, diatomite after coupling modification, glucose, and brassinolide into the stirring tank Carry out stirring, control the rotating speed of the stirring tank to be 400 rpm, the temperature of the stirring tank to be 30 ° C, and the stirring time to be 40 min. After the stirring, jet pulverization is performed, and the pulverization temperature during the control jet pulverization is 20 ° C, and the pressure when entering the jet pulverizer is 1.5MPa, the pulverization pressure is 3MPa, the airflow velocity is 250m / s, the pulverization time is 1.2h, and the primary mixture is obtained after the airflow pulverization;

[0041] Wherein, the weight ratio of pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, diatomite after coup...

Embodiment 2

[0061] A preparation method of a water-dispersible granule containing pyraclostrobin and dimethomorph, specifically:

[0062] 1. Preparation of a mixture: add pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, coupled and modified diatomite, glucose, and uniconazole into the stirring tank for stirring , the rotating speed of the control stirring tank is 450rpm, the temperature of the stirring tank is 32 ℃, and the stirring time is 42min, and after the stirring, jet pulverization is carried out, and the pulverization temperature during the control jet pulverization is 22 ℃, and the pressure when entering the jet pulverizer is 1.6MPa , the crushing pressure is 3.2MPa, the airflow velocity is 270m / s, the crushing time is 1.3h, and the primary mixture is obtained after the airflow crushing;

[0063] Among them, the weight ratio of pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, diatomite after coupling modification, glucose and ...

Embodiment 3

[0083] A preparation method of a water-dispersible granule containing pyraclostrobin and dimethomorph, specifically:

[0084] 1. Preparation of a mixture: add pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, diatomite after coupling modification, glucose, and gibberellin into the stirring tank for stirring , the rotating speed of the control stirring tank is 500rpm, the temperature of the stirring tank is 35 ℃, and the stirring time is 45min. After the stirring, jet pulverization is carried out. , the crushing pressure is 3.5MPa, the airflow velocity is 280m / s, the crushing time is 1.5h, and the primary mixture is obtained after the airflow crushing;

[0085] Among them, the weight ratio of pyraclostrobin, tea saponin, calcium lignosulfonate, modified disintegrant, diatomite after coupling modification, glucose and gibberellin is 130:6:6:8 :15:8:4.4;

[0086] The preparation method of the modified disintegrant is as follows: placing sodium tripolyp...

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Abstract

The invention discloses a preparation method of a water dispersible granule containing pyraclostrobin and dimethomorph, and belongs to the technical field of pesticides, the preparation method comprises the following steps: preparing a primary mixture, preparing a secondary mixture, and preparing the water dispersible granule containing pyraclostrobin and dimethomorph. According to the preparation method disclosed by the invention, the content of pyraclostrobin and dimethomorph in the water dispersible granule can be increased while the influence of high-temperature granulation and drying processes on the plant growth regulator is avoided and the disintegration property, the suspension rate and the suspension stability of the water dispersible granule are improved, so that the phytotoxicity generated after the water dispersible granule is used is avoided.

Description

technical field [0001] The invention relates to the technical field of pesticides, in particular to a preparation method of water dispersible granules containing pyraclostrobin and dimethomorph. Background technique [0002] Pyraclostrobin is a new type of broad-spectrum methoxy acrylic acid fungicide. It inhibits mitochondrial respiration and eventually leads to cell death. It has the functions of protection, treatment, and leaf osmotic conduction. It is mainly used to prevent smelting crops from fungi A variety of diseases caused by it, such as powdery mildew, scab, downy mildew, black rot, brown blight, branch blight, angular spot, anthracnose, fusarium wilt, etc. have better control effects. [0003] Dimethomorph is a new type of systemic therapeutic low-toxicity fungicide. Its mechanism of action is to destroy the formation of the bacterial cell wall membrane, causing the decomposition of the sporangium wall and causing the bacterial death. In addition to zoospore form...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/14A01N47/24A01N43/84A01N43/22A01N43/653A01N43/12A01N45/00A01N25/00A01N25/08A01P3/00A01P21/00
CPCA01N25/14A01N47/24A01N43/84A01N43/22A01N43/653A01N43/12A01N45/00A01N25/00A01N25/08Y02A50/30
Inventor 刘克贺金梁鹏郝严磊宋保远
Owner 山东百农思达生物科技有限公司
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