Synthetic fiber containing animal hair protein and manufacturing method thereof
A synthetic fiber and animal hair technology, applied in the direction of cellulose/protein conjugated artificial filament, conjugated synthetic polymer artificial filament, etc., can solve the problems of single use of fiber, poor stability of cystine, poor strength, etc. Achieve the effect of good elasticity and skin affinity, good strength and good air permeability
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Embodiment 1
[0015] Example 1: After degreasing and removing impurities, animal hair is soaked in an aqueous solution with a pH of 1.5 and stirred. After 6 hours at a temperature of 70°C, the waste residue is separated and purified, and the isoelectric point of the leachate is adjusted with alkali to obtain protein isolate. ; Dissolve the isolated protein in a soft aqueous solution containing sodium dodecylsulfonate, the dissolution temperature is 15°C, and the dissolution time is 4 hours to make a protein solution; add a certain amount of purified polyvinyl alcohol directly into the protein solution , to make them blend and copolymerize, the temperature is slowly raised to 98°C, and kept for 1.5 hours, during which soft water is added to adjust the concentration, and a spinning solution containing protein and polyvinyl alcohol with a concentration of 14% is obtained, wherein the protein and polyvinyl alcohol The weight ratio of dry solids is 3:97; adding boric acid to the spinning solution...
Embodiment 2
[0016] Example 2: After degreasing and removing impurities, animal hair is soaked in an aqueous solution with a pH of 2 and stirred. After 7 hours at a temperature of 40°C, the waste residue is separated and purified, and the isoelectric point of the leaching solution is adjusted with alkali to obtain isolated protein. ; Dissolve the isolated protein in a soft aqueous solution containing sodium dodecylsulfonate at a temperature of 30°C and a dissolution time of 2 hours to make a protein solution; add a certain amount of purified polyvinyl alcohol directly into the protein solution , to make them blend and copolymerize, the temperature is slowly raised to 98°C, and kept for 3.5 hours, during which soft water is added to adjust the concentration, and a spinning solution containing protein and polyvinyl alcohol with a concentration of 27% is obtained, wherein the protein and polyvinyl alcohol The weight ratio of dry solids is 60:40; adding boric acid to the spinning solution to ad...
Embodiment 3
[0017] Example 3: Soak human hair in an aqueous solution with a pH of 2.3 after degreasing and removing impurities, and stir it. After 4 hours at a temperature of 90°C, separate and purify to remove the waste residue, adjust the isoelectric point of the leachate with alkali, and obtain human hair Isolate protein; dissolve the isolated protein in a soft aqueous solution containing sodium dodecylsulfonate, the dissolution temperature is 60°C, and the dissolution time is 1.5 hours to make a protein solution; add a certain amount of washed pure polyvinyl alcohol directly to the protein In the solution, they are blended and copolymerized, and the temperature is slowly raised to 98 ° C, and kept for 2.5 hours, during which soft water is added to adjust the concentration, and a spinning solution containing protein and polyvinyl alcohol with a concentration of 38% is obtained, wherein protein and polyethylene The weight ratio of alcohol to dry solids is 45:55; add boric acid to the spi...
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