Pulping method of non-wood fibers with no black liquor drained off as well as its boiler

A non-wood fiber and digester technology, which is applied in the direction of cellulose raw material pulping, digester, and fiber raw material treatment, can solve problems such as bleaching difficulties, adverse environmental effects, and recycling troubles, and achieve simple and easy process and reduce Effects of washing water consumption, easy separation and dehydration

Inactive Publication Date: 2003-10-01
SHENGBANG SCI & TECH MIANYANG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Such pulping method has the following problems: due to the use of sodium sulfide agent, malodorous gases such as hydrogen sulfide, mercaptan, and sulfur dioxide will be produced during cooking, which will have a serious impact on the atmospheric environment; due to the use of high-temperature and high-pressure cooking, lignin will deteriorate. As a result, bleaching is difficult. In order to obtain pulp with high brightness, multi-stage bleaching with chlorine bleaching agent is required. In this process, harmful substances such as organic chlorides will be generated, which will seriously affect the water environment; a large amount of alkali and other agents are used for cooking. , needs to be recovered from the black liquor. For this reason, the black liquor needs to be concentrated, burned, causticized, etc., which requires the use of complex and huge equipment, resulting in increased equipment investment costs; at the same ti

Method used

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  • Pulping method of non-wood fibers with no black liquor drained off as well as its boiler
  • Pulping method of non-wood fibers with no black liquor drained off as well as its boiler
  • Pulping method of non-wood fibers with no black liquor drained off as well as its boiler

Examples

Experimental program
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Example Embodiment

[0033] Example one:

[0034] Indicator name

[0035] Add 3.6 kg of Jilin-produced reed (moisture content 13.63%) into a stainless steel digester with a screen and a jacket, and add 32 kg of acetic acid with a concentration of 906g / L (50ml of concentrated sulfuric acid is added in advance). Steam for 120 minutes at ℃. Use the pressure in the digester to transfer the black hydraulic pressure into the waste acid storage tank. Then add 12 kilograms of 90% ethanol to the digester, perform acid alcohol digestion at 110-120°C for 60 minutes, and use the pressure in the digester to push the black hydraulic pressure into the spent acid alcohol liquid storage tank. Then the pulp is washed with hot alcohol solution and then with hot water. The washing method is the same as that in the preparation of bamboo pulp, except that the amount of alcohol is 12 kg each time.

[0036] Indicator name

[0037] Indicator name

[0038] Indicator name

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Abstract

A process for preparing the pulp of non-woven fibres without black liquid drainage includes such steps as adding raw fibres and acetic acid into the enclosed digester, heating, holding the temp for acertain time, filtering to obtain waste acidic liquid, pumping it to waste acid tank, adding the washing alcohol solution, heating, holding the temp for a certain time, filtering the waste acid-alcohol solution, pumping it to waste acid-alcohol tank, washing fibres with clean alcohol, draining the washing liquid to waste liquid tank, stripping alcohol from fibres by low-pressure steam, adding hotwater to digester, and discharging raw pulp. Said digester has a jacket with steam inlet and condensed water outlet and a filter net at the discharge port.

Description

1. Technical field [0001] The invention relates to a papermaking pulping method and equipment thereof, in particular to joint cooking of non-wood fiber raw materials with acetic acid and ethanol, so that lignin and part of hemicellulose are dissolved in cooking liquid and separated from cellulose. Utilizing the characteristics that these solvents in the black liquor are easy to volatilize, they can be recovered by distillation and recycled. The lignin and hemicellulose are collected in the form of solids, thus realizing the emission of no black liquor and odorous gases such as hydrogen sulfide and mercaptan. Clean the pulping process and the corresponding digesters. 2. Background technology [0002] The two existing chemical pulping methods: kraft method and sulfite method have not changed much since they were developed more than one hundred years ago. As far as the representative kraft method of chemical pulping is concerned, the general process is: add fiber raw materials...

Claims

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Application Information

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IPC IPC(8): D21C3/00D21C7/00
Inventor 聂庆伟
Owner SHENGBANG SCI & TECH MIANYANG
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