New CuI Crystal and growing method thereof
A new type of crystal technology, applied in the field of CuI crystal growth, achieves the effect of simple equipment, low growth temperature and low price
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[0014] Analytical pure sodium silicate, ionized water, and acetic acid were selected as raw materials for preparing the gel, analytically pure hydroiodic acid was used as a complexing agent, and CuI powder was used as a raw material to grow CuI crystals. Dissolve 106 grams of sodium silicate in 250 grams of deionized water, and filter after completely dissolving. Further dilute the above sodium silicate aqueous solution with deionized water, and add 2M acetic acid, the volume ratio of sodium silicate aqueous solution, deionized water, and acetic acid is 7:8:15 (such as 70ml sodium silicate, 80ml deionized water, 150ml acetic acid), stirring constantly during the solution preparation process. The prepared solution was poured into a U-shaped tube with a diameter of 3 cm, a height of 25 cm, and a width of 20 cm. After standing at a temperature of 25±0.5° C. for 48 hours, a gel for crystal growth was formed.
[0015] Dissolve CuI powder in different amounts of 7M hydriodic acid t...
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