Rare-earth forage additive prepn. method and use thereof
A feed additive and rare earth technology, applied in animal feed, animal feed, applications, etc., can solve the problems of not showing the advantages of promoting growth, it is difficult to determine the appropriate amount of addition, and the ingredients vary greatly, so as to improve the quality of animal products, Improve feed utilization efficiency and reduce cost
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Embodiment 1
[0025] 1) Put the commercially available 001×7 strong acidic styrene-based cation exchange resin (this product is equivalent to the United States: AmberrliteIR-120Dowex-50, West Germany: Lewatit-100, Japan: DiaonSK-1), and place it in the same volume as the resin Soak in 0.5mol / L hydrochloric acid solution for 6 hours, drain the acid solution and rinse with water until neutral;
[0026] 2) Pre-configure lanthanum chloride containing 0.5% by weight of the cation exchange resin into a 0.1 mol / L aqueous solution, slowly add it to the resin in step 1) under stirring, detect and adjust the pH value of the reaction solution to 3.5 , react at room temperature for 5 hours;
[0027] 3) In the detection step 2) the pH value of the reaction solution is adjusted with an aqueous sodium hydroxide solution with a concentration of 10moL / L, so that the pH value of the reaction solution is 7.0; washed 3 times with water, filtered and dehydrated;
[0028] 4) drying and pulverizing the filter ca...
Embodiment 2
[0030] 1) Soak the commercially available D001 macroporous strongly acidic styrene-based cation conversion resin (this product is equivalent to America: Amberlite200, West Germany: Lewaitet-SP120) in a 5mol / L hydrochloric acid solution 4 times the volume of the resin for 3 hours, After draining the acid solution, rinse with water until neutral;
[0031]2) terbium nitrate whose terbium content is 1% by weight of the cation exchange resin and yttrium chloride whose yttrium content is 1% by weight of the cation exchange resin are pre-configured into a 2.0mol / L aqueous solution, and slowly added to the resin of step 1) under stirring , detect and adjust the pH value of the reaction solution to 6.5, and react at room temperature for 10 hours;
[0032] 3) In detection step 2) the pH value of the reaction solution is adjusted with an aqueous potassium hydroxide solution with a concentration of 0.5moL / L, so that the pH value of the reaction solution is 8.5; washed 6 times with water, ...
Embodiment 3
[0035] 1) Put the commercially available 001×12 / 14 / 16 strongly acidic styrene-based cation exchange resin (this product is equivalent to the US: Amberlite IR-132, IR-130, IR-124) in 3mol of 1.5 times the volume of the resin Soak in / L hydrochloric acid solution for 3 hours, drain the acid solution and rinse with water until neutral;
[0036] 2) lanthanum chloride whose lanthanum content is 1% by weight of the cation exchange resin, cerium nitrate whose cerium content is 1% by weight of the cation exchange resin, praseodymium chloride whose content of praseodymium is 0.5% by weight of the cation exchange resin, and cation exchange resin whose content of neodymium is 0.5% by weight of neodymium nitrate, pre-configured into a 1.0mol / L aqueous solution, slowly added to the resin in step 1) under stirring, the pH value of the reaction solution was detected and adjusted to 5.0, and reacted at room temperature for 8 hours;
[0037] 3) The pH value of the detection step 2) is adjusted...
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