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Method for producing bamboo pomace

A technology of bamboo pulp and bamboo material, which is applied in pulp bleaching, pulping with inorganic alkali, pulping of cellulose raw materials, etc., can solve problems such as difficult quality control, large fluctuations in product quality, complicated production methods, etc. Effect of hydrolysis and cooking, reduction of process steps, and effect of accelerated dissolution rate

Active Publication Date: 2010-10-13
吉林化纤股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Due to the contradiction between the increase of whiteness and the decrease of polymerization degree in the bleaching process, the prior art generally adopts three-stage bleaching or four-stage bleaching to achieve certain effects.
[0007] However, the status of the prior art often has the problems of many steps, large consumption and serious pollution because of the above-mentioned pretreatment and bleaching processes. For a more representative technical solution, please refer to the disclosed "a kind of using bamboo material" in Chinese patent application CN1308160. The process of producing viscose fiber pulp", the technological process adopted is: material preparation→cutting→screening→washing→prehydrolysis→washing→cooking→dumping→washing→screening→thawing→sand removal→concentration→ Chlorination, washing → alkali refining, washing → bleaching, washing → acid treatment → washing → desanding → concentration → papermaking; after cooking, the content of Type A cellulose is ≥ 95.5%, and the hardness of the pulp (kapoise value) 4-10, the average degree of polymerization DP≥600; pulp whiteness after bleaching≥75%, the average degree of polymerization DP≥450, viscosity≥7.5mPa·s, cellulose content of class A≥93%
The production method of this technical solution is complicated, the process flow is long, the energy consumption is high, the pollution is serious, the quality control is difficult, the product quality fluctuates greatly, and it is difficult to meet the needs of actual production development.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Slice the bamboo according to the cross-section. The cross-section and the bamboo axis form an angle of 60 degrees. The distance between the slices is 20mm. It is a horseshoe-shaped sheet. Put steamed balls and add water. , Keep for 150 minutes; then discharge the hydrolyzate. Add NaOH and Na to the steamer 2 For the mixed solution of S, the amount of NaOH is 20% of the dry raw material weight, the degree of sulfidation is 25.0%, the liquid ratio is 1:3.5, the holding pressure is 0.65MPa, the holding time is 150 minutes, and the cooking is completed to obtain a slurry.

[0035] The obtained slurry is desanded in the desander, the desanding slurry concentration is 0.7%, the desanding pressure is 0.30MPa, and then bleached in the bleaching tank; a one-stage bleaching process is adopted, at an alkali content of 60g / m 3 Under certain conditions, the temperature is 45°C, the bleaching time is 30 minutes, and the bleaching chlorine content is 0.2g / L; the pulp after bleaching...

Embodiment 2

[0038]Slice the bamboo according to the cross-section. The cross-section and the bamboo axis form an angle of 40 degrees. The distance between the slices is 25mm. It is a horseshoe-shaped sheet. Put it into a vertical steamer and add water. 0.75Mpa, keep for 100 minutes; then discharge the hydrolyzate. Add lye into the steaming ball, the alkali is NaOH, the amount of alkali used is 30% of the dry raw material weight, the liquid ratio is 1:4, the holding pressure is 0.75MPa, the holding time is 100 minutes, and the cooking is completed to obtain a slurry.

[0039] The obtained slurry is desanded in the desander, the desanding slurry concentration is 0.8%, the desanding pressure is 0.25MPa, and then bleached in the bleaching tank, adopting a one-stage bleaching process, and the bleaching alkali contains 150g / m 3 , the temperature is 40°C, the bleaching time is 100 minutes, and the bleaching chlorine content is 0.40g / L; the pulp after bleaching is treated with hydrochloric acid, ...

Embodiment 3

[0042] Slice the bamboo according to the cross-section. The cross-section and the bamboo axis form an angle of 50 degrees. The distance between the slices is 40mm. It is a horseshoe-shaped sheet. Put steamed balls and add water. , keep for 120 minutes; then discharge the hydrolyzate; add Na to the steaming ball 2 O and Na 2 For the mixed solution of S, the amount of alkali used is 25% of the dry raw material weight, the degree of sulfidation is 20.0%, the liquid ratio is 1:3.8, the heat preservation pressure is 0.70 MPa, heat preservation is 120 minutes, and the cooking is completed to obtain a slurry.

[0043] The obtained slurry is desanded in a desander, the desanding slurry concentration is 0.75%, and the desanding pressure is 0.20Mpa. Then bleach in the bleaching tank, using a one-stage bleaching process, bleaching contains 120g / m of alkali 3 Under certain conditions, the first-stage bleaching temperature is 42°C, the bleaching chlorine content is 0.30g / L, and the bleac...

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PUM

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Abstract

The present invention provides a preparation method of bamboo pulp, belonging to the field of chemical fiber technology. Said method includes the following steps: obliquely cutting bamboo strip material into the form of horseshoe, the chip cross-section spacing distance is 20-40 mm, then prehydrolyzing the prepared bamboo strip, adding alkali and cooking, removing sand, making one-stage or two-stage bleaching treatment, making the bleached pulp material undergo the processes of acid treatment, concentration and pulping so as to obtain the invented bamboo pulp. Said bamboo pulp can be used forproducing viscose fibre.

Description

technical field [0001] The invention relates to a preparation method of bamboo pulp, which belongs to the technical field of chemical fibers. Background technique [0002] As a raw material for the textile industry, chemical fibers are developing day by day, especially in today's increasingly scarce energy sources. The manufacture of chemical fibers is largely limited by coal and petroleum resources, so people have to turn their attention back to cellulose fibers in search of raw materials for making fibers. [0003] Bamboo has very rich resources in our country and is widely distributed. There are more than 40 genera and more than 400 varieties of bamboo. After planting and surviving, they can be cut down in 2-3 years. It is a fast-growing and high-yielding plant material. Taking the most widely used and better quality Cizhu as an example, its comprehensive cellulose content is 40-50%, lignin content is 20-30%, ash content is 1-3%, polypentose is 16-20%, fiber The average...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D21C3/00D21C3/02D21B1/06D21C1/04D21C1/10D21C7/00D21C9/02D21C9/12
Inventor 宋德武郑书华岳福升李振峰孙同会薛振军范梅欣张焕志
Owner 吉林化纤股份有限公司
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