Flame-retardant epoxy resin composition
一种环氧树脂、组合物的技术,应用在运输和包装、印刷电路、薄料处理等方向,能够解决无法表现出阻燃性等问题,达到优异耐热性的效果
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preparation example Construction
[0046] The preparation of component (A) can also be carried out in the presence of a suitable solvent capable of dissolving component (A). If a solvent is used, preferred examples include inert solvents such as N,N-dimethylformamide, N,N-diethylformamide, N-methyl-2-pyrrolidone, dimethylsulfoxide, methylethyl Ketones, xylene, toluene, methyl cellosolve, tetrahydrofuran, etc. These solvents may be used alone or in combination of two or more.
[0047] In the preparation of component (A), a predetermined amount of epoxy resin raw material is charged into a reaction vessel, and then the reaction vessel is heated and adjusted at a prescribed temperature. Next, the catalyst is added mixed with water or a suitable solvent. The addition of the catalyst is carried out at a temperature ranging from 20°C to 200°C, preferably at 80°C to 200°C, more preferably at 110°C to 180°C. It is preferable to add the catalyst at a temperature greater than or equal to 20°C, because the reaction bet...
preparation example 1
[0095] 0.04 parts of tetrabutylammonium bromide were added to 100 parts of bisphenol A epoxy resin (epoxy equivalent: 189 g / equivalent). The resulting solution was heated with stirring to an internal temperature of 175°C. To this solution was added 16.1 parts of Coronate T-80 over a period of 120 minutes TM (TDI, manufactured by Nippon Polyurethane Industry Co., Ltd.; approximately 80% of 2,4-toluene diisocyanate, approximately 20% of 2,6-toluene diisocyanate). Immediately after the addition was complete, the resulting solution was stirred for 4 hours while maintaining the reaction temperature at 175° C., thereby obtaining epoxy resin I containing an oxazolidinone ring.
preparation example 2
[0097] 0.04 parts of tetrabutylammonium bromide were added to 100 parts of bisphenol A epoxy resin (epoxy equivalent: 189 g / equivalent). The resulting solution was heated with stirring to an internal temperature of 175°C. To this solution was added 30.9 parts of MR-200 over a period of 120 minutes TM (diphenylmethane diisocyanate manufactured by Nippon Polyurethane Industry Co., Ltd.). Immediately after the addition was complete, the resulting solution was stirred for 4 hours while maintaining the reaction temperature at 175° C., thereby obtaining epoxy resin II containing an oxazolidinone ring.
[0098] The properties of epoxy resins I and II containing oxazolidinone rings are shown in Table 1. In Table 1, "n=0 component" means an unreacted monomer component in the bisphenol A type epoxy resin raw material.
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