The invention discloses a
phosphorus-doped double-vacancy heterostructure material, a preparation method and application, and belongs to the technical field of electrocatalysis, polyacid is used as a precursor to prepare P-MoS2 rich in
sulfur vacancies on carbon cloth through
hydrothermal treatment, then part of MoS2 is converted into MoO2 in situ through heat treatment, and a P-MoS2 / MoO2 heterostructure is constructed. Abundant
oxygen vacancies are generated in the thermal conversion process. Rich vacancy defects and heterogeneous interfaces in the constructed catalyst promote
electron transfer and adsorption of active substances, charge transfer
kinetics is improved, and more reaction active sites are provided for water
cracking; the vertically crossed
nanosheet network on the carbon cloth is beneficial to charge transport, reactant
permeation and gas
diffusion. Various components in the catalyst synergistically promote the water
electrolysis process, and a novel advanced, economical, efficient and stable
electrode material is provided for catalytic application.